User Manual

<5. CALIBRATION OF pH/ORP>
5-1
IM 12A01A02-01E 5th Edition : Oct. 31, 2013-00
5. CALIBRATION OF pH/ORP
BeforepHmeasurement,calibratethepHsensorwiththestandardsolution.
BeforeORPmeasurement,checktheelectrodeasapartofregularmaintenance.
NOTE
A default is “10 min” for “Auto Return”. When maintenance like a calibration that may take much
timeisperformed,“60min”or“Disable”isrecommendedtobeselected. (Refer to the section
4.7.3.)
Calibration
Execute:
Calibration
HOLD
Temporary output
Setup:
Commissioning
Change language
Start Quick Setup
Execute & Setup Calibration pH
pH
ORP
Temperature
Manual
Automatic
Sample
Temperature calibration
or
Only when “pH + ORP” is selected
on the Sensor setup screen
Figure 5.1 Calibration
The calibration items include pH, ORP, rH, and Temperature.
The item to be calibrated is determined according to the settings made in the Sensor setup and
Measurement setup in Commissioning.
Press
toselectExecute:Calibration,choosetheitemtobecalibrated,congurethe
calibration settings, then perform calibration.
NOTE
Notethefollowingwhenperformingcalibrationwithbuffersolutions.
1. Beforestartingacalibration,makesuretheelectrodesystemisproperlycleanedand
the electrodes are fully functional. They must then be rinsed with clean water to avoid
contamination of the calibration solution(s).
2. Always use fresh buffer solution to avoid the risk of introducing errors from contaminated or
oldsolutions.Bufferssuppliedasliquidshavealimitedshelflife,especiallyalkalinebuffers,
which absorb CO
2
from the air.
3. YokogawastronglyrecommendsNIST/DIN19266bufferstandardsforthebestaccuracy
and buffer capacity. Commercially adjusted buffers (e.g., pH 7.00, 9.00 or 10.00) are a
compromise as a standard, and are often supplied without a temperature dependency
curve.TheirstabilitywillneverbeasgoodasNIST(JISequivalent)solutions.
Alwaysensurethatthesensorsareproperlyconditioned,cleanandlledwiththecorrect
electrolyte solution (if appropriate) before starting a calibration. Refer to the sensor instructions
for details.
PH
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