858 Professional Sample Processor Manual 8.858.
Metrohm AG CH-9100 Herisau Switzerland Phone +41 71 353 85 85 Fax +41 71 353 89 01 info@metrohm.com www.metrohm.com 858 Professional Sample Processor Manual 8.858.8002EN 06.
Teachware Metrohm AG CH-9100 Herisau teachware@metrohm.com This documentation is protected by copyright. All rights reserved. Although all the information given in this documentation has been checked with great care, errors cannot be entirely excluded. Should you notice any mistakes please send us your comments using the address given above. Documentation in additional languages can be found on http://products.metrohm.com under Literature/Technical documentation.
■■■■■■■■■■■■■■■■■■■■■■ Table of contents Table of contents 1 Introduction 1 1.1 Field of application ............................................................... 1 1.2 Instrument description ......................................................... 1 1.3 Model versions ...................................................................... 2 1.4 Intended use ......................................................................... 3 1.5 About the documentation .................................
■■■■■■■■■■■■■■■■■■■■■■ Table of contents 3.10 Connecting the tower stirrer ............................................. 28 3.11 Connecting pumps ............................................................. 29 3.12 Installing the peristaltic pump .......................................... 30 3.13 Connecting a computer ...................................................... 33 3.14 Connecting MSB devices ................................................... 35 3.14.1 Connecting dosing devices .......
■■■■■■■■■■■■■■■■■■■■■■ Table of contents 8 Conformity and warranty 52 8.1 Declaration of Conformity ................................................. 52 8.2 Quality Management Principles ........................................ 53 8.3 Warranty (guarantee) ......................................................... 54 9 Accessories 55 9.1 Scope of delivery ................................................................ 55 9.1.1 858 Professional Sample Processor 2.858.0010 .....................
■■■■■■■■■■■■■■■■■■■■■■ Table of figures Table of figures Figure 1 Figure 2 Figure 3 Figure 4 Figure 5 Figure 6 Figure 7 Figure 8 Figure 9 Figure 10 Figure 11 Figure 12 Figure 13 Figure 14 Figure 15 Figure 16 Figure 17 Figure 18 Figure 19 Figure 20 Figure 21 Figure 22 Figure 23 Figure 24 Figure 25 Figure 26 Figure 27 Figure 28 Figure 29 Figure 30 Figure 31 Figure 32 Figure 33 Figure 34 Figure 35 Figure 36 Figure 37 Figure 38 Figure 39 Figure 40 Figure 41 Figure 42 VI ■■■■■■■■ Front 858 Professional Sampl
■■■■■■■■■■■■■■■■■■■■■■ 1 Introduction 1 Introduction 1.1 Field of application The 858 Professional Sample Processor is an instrument with many applications that was conceived for preparing samples for ion chromatography. Inline filtration, dialysis, preparing dilutions, sample preconcentration, inline calibration, partial loopfill, etc. are techniques that can be used with the 858 Professional Sample Processor without any problem.
■■■■■■■■■■■■■■■■■■■■■■ 1.3 Model versions 1.3 Model versions The 858 Professional Sample Processor is available in various models with a number of different accessories. Table 1 Model versions of the 858 Professional Sample Processor Model 2.858.0010 ■ ■ ■ ■ ■ ■ Tower with 786 Swing Head and robotic arm 2 pump connectors 1 stirrer connector 3 connectors for dosing devices and/or stirrers 2 USB connectors Controller connection for connection to PC Model 2.858.
■■■■■■■■■■■■■■■■■■■■■■ 1.4 1 Introduction Intended use The 858 Professional Sample Processor is designed for usage as an automation system in analytical laboratories. It is not suitable for usage in biochemical, biological or medical environments in its basic equipment version. This instrument is suitable for processing chemicals and flammable samples.
■■■■■■■■■■■■■■■■■■■■■■ 1.6 Safety instructions Warning This symbol draws attention to a possible hazard due to heat or hot instrument parts. Warning This symbol draws attention to a possible biological hazard. Caution This symbol draws attention to a possible damage of instruments or instrument parts. Note This symbol marks additional information and tips. 1.6 Safety instructions 1.6.
■■■■■■■■■■■■■■■■■■■■■■ 1 Introduction Warning Never open the housing of the instrument. The instrument could be damaged by this. There is also a risk of serious injury if live components are touched. There are no parts inside the housing which can be serviced or replaced by the user. Mains voltage Warning An incorrect mains voltage can damage the instrument. Only operate this instrument with a mains voltage specified for it (see rear panel of the instrument).
■■■■■■■■■■■■■■■■■■■■■■ 1.6 Safety instructions Warning Always install the safety shield supplied with the equipment before using the instrument for the first time. Pre-installed safety shields are not allowed to be removed. The 858 Professional Sample Processor may not be operated without a safety shield! Warning Personnel are not permitted to reach into the working area of the instrument while operations are running! A considerable risk of injury exists for the user.
■■■■■■■■■■■■■■■■■■■■■■ 1.7 1 Introduction Recycling and disposal This product is covered by European Directive 2002/96/EC, WEEE – Waste from Electrical and Electronic Equipment. The correct disposal of your old equipment will help to prevent negative effects on the environment and public health. More details about the disposal of your old equipment can be obtained from your local authorities, from waste disposal companies or from your local dealer.
■■■■■■■■■■■■■■■■■■■■■■ 2.1 Front 2 Overview of the instrument 2.1 Front 1 5 2 6 7 8 3 4 s w i s s m Figure 1 a d e Front 858 Professional Sample Processor 1 Guide chain 2 Safety shield 3 Sample rack 4 Assembly rail 5 Peristaltic pump Depending on the model version 6 Swing Head 7 Injection valve Depending on the model version 8 Robotic arm with needle adapter (6.1462.
■■■■■■■■■■■■■■■■■■■■■■ 2.2 2 Overview of the instrument Rear 4 Ext. Pump 1 1 2 5 Swing Head WARNING - Fire Hazard with the same type and rating of fuse f: 50 - 60 Hz Contr. MSB 2 Nr. USB 1 U: 100 - 240 V Made by Metrohm Herisau Switzerland USB 2 3 P: 115W MSB 1 For continued protection replace only Figure 2 Ext.
■■■■■■■■■■■■■■■■■■■■■■ 2.3 Connector strip Connector strip 1 2 WARNING - Fire Hazard - 3 with the same type and rating of fuse U: 100 - 240 V 5 f: 50 - 60 Hz Made by Metrohm Herisau Switzerland USB 2 Figure 3 P: 115W MSB 1 For continued protection replace only USB 1 4 Contr. MSB 2 MSB 3 Nr. 2.3 Connector strip 858 Professional Sample Processor 1 USB connectors 2 Controller connector For the connection to the PC 3 MSB connectors For dosing devices, stirrers, etc.
■■■■■■■■■■■■■■■■■■■■■■ 2 Overview of the instrument Figure 5 Attaching a sample rack Certain sample racks have a handle with a fixing screw. With this, the rack can be fixed on the turntable by rotating in clockwise direction. Note After the sample rack has been attached, the rack must be initialized with the Rack initialization function in the control software ("Manual Operation"), so that the magnet code of the rack can be recognized.
■■■■■■■■■■■■■■■■■■■■■■ 2.5 The Swing Head Other user-defined racks can be supplied upon request and the required rack data can be defined in the control software. Any arrangement of rack positions is possible. The magnet code for user-defined racks is 110000. Magnet codes Every single sample rack can be unambiguously identified by means of a magnet code. Magnetic pins in a holder attached on the underside of the rack can be combined to make a binary, six-digit code.
■■■■■■■■■■■■■■■■■■■■■■ 2 Overview of the instrument 1 2 3 4 5 Figure 6 Swing Head - Configuration data 1 Swing axis This runs through the middle of the Swing Head drive. 2 Swing radius This is determined by the length of the robotic arm. The radius runs from the axis of rotation to the midpoint of the tip of the robotic arm. 3 Source axis This runs from the swing axis to the midpoint of the sample rack and marks the initial position of the robotic arm.
■■■■■■■■■■■■■■■■■■■■■■ 2.6 Peristaltic pump If a Swing Head drive is mounted with a 6.2058.020 adapter in order to use racks smaller than intended, then the axial distance must be modified in the configuration of the control software. The corresponding data can be found on the accompanying sheet of the 6.2058.020. The axial distance refers to the distance of the swing axis (see figure) and of the axis of rotation (middle point) of the sample rack. 2.
■■■■■■■■■■■■■■■■■■■■■■ 2.7 2 Overview of the instrument Injection valve The injection valve (for the model version 2.858.0030) can be used with its connectors 1 to 6 (see figure) for complex sample preparation steps. Figure 8 Injection valve The connections of the connectors in the switching positions FILL and INJECT can be found in the schematics shown below.
■■■■■■■■■■■■■■■■■■■■■■ 3.1 Setting up the instrument 3 Installation 3.1 Setting up the instrument 3.1.1 Packaging The instrument is supplied in highly protective special packaging together with the separately packed accessories. Keep this packaging, as only this ensures safe transportation of the instrument. 3.1.2 Checks Immediately after receipt, check whether the shipment has arrived complete and without damage by comparing it with the delivery note. 3.1.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation If the Swing Head is not connected, connect it as follows: 1 Plug in the cable Guide the Swing Head connection cable through the guide chain of the tower (see Chapter 3.7, page 23) and plug the Mini DIN plug into the 'Swing Head' socket. 3.3 Connecting the mains cable Warning This instrument may only be used with the mains voltage specified (see rear of the instrument). Protect the connection sockets against moisture. U: 100 - 240 V f: 50 - 60 Hz Nr.
3.5 Mounting a filtration cell holder or Dosino holder Figure 12 ■■■■■■■■■■■■■■■■■■■■■■ Mounting the retaining plate 1 Mount the retaining plate Fix the plate to the front of the tower with the four hexagon screws provided. The hexagon key required is part of the accessories. 3.5 Mounting a filtration cell holder or Dosino holder Figure 13 Mounting filtration cell holder or Dosino holder The filtration cell holder (6.2057.030) or the Dosino holder (6.2057.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation Figure 14 Mounting the Dosino Mount the Dosino as follows: 1 Fix the Dosino ■ ■ ■ Guide the thread adapter GL 45 (6.1618.020) from below into the Dosino holder. Attach the dosing unit on the Dosino holder and screw the thread adapter tight. Connect the tubings. Figure 15 858 Professional Sample Processor 6.1618.
■■■■■■■■■■■■■■■■■■■■■■ 3.6 Mounting the stand plate 3.6 Mounting the stand plate An external dilution or measuring cell can be mounted to the 858 Professional Sample Processor with the aid of a 6.2001.070 stand plate. Figure 16 6.2001.070 stand plate Mount the stand plate as follows: 1 Mount the support rod ■ ■ ■ Plug together the cutting ring and the hexagon screw with the base plate (see below) and place on a flat support surface. Place the support rod on the screw and screw tightly.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation 2 Fasten the stand plate ■ ■ Hook the fixing clamps on the stirrer rail. Tighten the hexagon screws of the fixing clamps. Figure 18 Mounting the stand plate 3 Mount the stirrer and dilution vessel ■ ■ ■ ■ 858 Professional Sample Processor Hang the magnetic stirrer (801 Stirrer) on the support rod and align it. Fix the orientation of the stirrer using the red knurled screw on the rear. Fasten the 6.2013.010 clamping ring, see the following figure.
■■■■■■■■■■■■■■■■■■■■■■ 3.6 Mounting the stand plate Figure 19 Mounting the stirrer and the dilution vessel 4 Mount the cross strut ■ ■ Assemble the cross strut according to the drawing shown below. Fasten the cross strut provisionally to the support rod. Figure 20 Mounting the cross strut 5 Fix the support rod ■ ■ 22 ■■■■■■■■ Screw the cross strut to the rear of the tower with the hexagon screw provided as shown below. Tighten all hexagon screws.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation Figure 21 Fixing the support rod The accessories for the dilution vessel and the necessary tubings and capillaries can then be attached. You will find information about the corresponding accessories set in the documentation. 3.7 Guide chain for cables and tubing Tubing, capillaries and cables can be placed in the guide chain. You can open the individual chain links with a screwdriver as follows.
■■■■■■■■■■■■■■■■■■■■■■ 3.7 Guide chain for cables and tubing Figure 22 Guide chain - Opening chain links 2 Insert into the guide chain ■ Place the required tubing, capillaries or cables into the guide chain. 3 Close the guide chain ■ Close the clip for each chain link again by hand and apply forceful pressure to snap them into place. The clip of one chain link can be removed entirely if required by releasing it on both sides.
■■■■■■■■■■■■■■■■■■■■■■ 3.8 3 Installation Mounting the sample tube Needles made of zirconium oxide or PEEK can be used for removing samples. Warning When a sample tube 6.1835.050 or a blunt PEEK needle is used, no stopper is permitted to be used on the sample vessels. These stoppers cannot be penetrated by such needles. The needle could become damaged if this is attempted! Perforated stoppers can be used with double-bevel needles. 1 2 3 4 5 6 Figure 23 1 Mounting the needle PTFE capillary 6.1803.
■■■■■■■■■■■■■■■■■■■■■■ 3.8 Mounting the sample tube 3 Nut 4.766.4320 (or 6.2833.020 + 6.2744.080) 4 Ring wedge 5 Needle holder 6 Sample tube 6.2846.000 (zirconium oxide) or 6.1835.020 / 6.1835.040 / 6.1835.050 (made of PEEK) This is how you mount needle and capillary: 1 Remove the PEEK pressure screw Loosen and remove the nut (23-3) screwed onto the needle holder. 2 Insert the needle ■ ■ Insert the needle from above part way into the opening of the needle holder (23-5).
■■■■■■■■■■■■■■■■■■■■■■ 3.9 3 Installation Mounting the safety shield For safety reasons, it is imperative that you mount the accompanying safety shield (splash protection 6.2751.110). A serious risk of injury exists if anyone reaches into the working area of the instrument. Caution The 858 Professional Sample Processor may not be operated without a safety shield. Use the accompanying hexagon screws and the hexagon key to mount the safety shield according to the following figure.
■■■■■■■■■■■■■■■■■■■■■■ 3.10 Connecting the tower stirrer 3.10 Connecting the tower stirrer A DIN socket for connecting a rod stirrer (802 Stirrer) or a magnetic stirrer (741 Stirrer) is located on the rear of the tower. Figure 25 Rod stirrer 802 Stirrer Figure 26 Magnetic stirrer 741 Stirrer Take care to observe correct orientation of the contact pins when plugging in the stirrer connection cable. The rib on the outside of the plug must match the reference mark (on the left) on the socket.
■■■■■■■■■■■■■■■■■■■■■■ 3.11 3 Installation Connecting pumps The 858 Professional Sample Processor is equipped with two connectors for external pumps which, for example, can be used for rinsing or applying suction to vessels. The appropriate pump models are: Figure 28 772 Pump Unit The peristaltic pump 772 Pump Unit is suitable for organic solvents and aqueous solutions containing precipitates.
■■■■■■■■■■■■■■■■■■■■■■ 3.12 Installing the peristaltic pump The two pump connectors are located on the rear side of the tower. Connect a pump as follows: 1 Connecting the connection cable ■ ■ Plug the M8 plug of the pump connection cable into one of the "Ext. Pump" connector sockets. Correct orientation of the 3 contact pins must be observed. Tighten the knurled screw at the front end of the plug by hand in clockwise direction. This will secure the plug.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation Mount the pump tubing as follows: 1 Remove the tubing cartridge Release the tubing cartridge from the cartridge holder by pressing the snap-action lever and unhooking from the mounting bolts (see Figure 7, page 14). 2 Insert the pump tubing ■ ■ Press the contact pressure lever all the way down. Place the pump tubing in the tubing cartridge. The stoppers (31-3) must snap into the corresponding holder of the tubing cartridge. 3 Connect the aspiration side Place a 6.
■■■■■■■■■■■■■■■■■■■■■■ 3.12 Installing the peristaltic pump Figure 32 Inserting the tubing cartridge 6 Connect the capillaries ■ Screw the respective capillaries tightly to the two tubing olives with PEEK pressure screws (31-1). Setting the flow rate The contact pressure of the tubing cartridge must be adjusted in order to regulate the flow rate. Proceed as follows: 1 Set the contact pressure ■ ■ ■ ■ Press the contact pressure lever (31-5) all the way forward.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation The flow rate depends not only on the correct contact pressure but also on the inner diameter of the pump tubing and the rotational speed of the drive. Note Pump tubings are consumables. The lifetime of the pump tubings depends on the contact pressure, among other factors. 3.13 Connecting a computer The 858 Professional Sample Processor requires a USB connection to a computer in order to be able to be controlled by a PC software. Using a 6.2151.
■■■■■■■■■■■■■■■■■■■■■■ 3.13 Connecting a computer USB 2 6.2151.000 Figure 33 USB 1 Contr. MSB 2 Connecting the computer The instrument is recognized. The driver installation is carried out differently, depending on the version of the Windows operating system used. ■ Either the required driver is installed automatically, or an installation wizard is started. 3 Follow the instructions of the installation wizard. If problems should occur during installation, contact your company's IT supporter.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation More detailed information concerning the configuration of the instrument can be found in the documentation for the respective PC software. 3.14 Connecting MSB devices In order to connect MSB devices, e.g.stirrers or dosing devices, Metrohm instruments are equipped with up a maximum of four connectors at what is referred to as the Metrohm Serial Bus (MSB).
■■■■■■■■■■■■■■■■■■■■■■ 3.14 Connecting MSB devices Note When connecting MSB devices together, the following must be observed: ■ ■ ■ ■ Only one device of the same type can be used at a single MSB connector at one time. Type 700 Dosino and 685 Dosimat dosing devices cannot be connected together with other MSB instruments on a shared connector. These dosing devices must be connected separately. Only one device of the same type can be used at a single MSB connector at one time.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation Warning If a Dosino is connected to the 858 Professional Sample Processor then the connection cable must be equipped with a T.2400.102 ferrite core. The ferrite core reduces any interference voltages that may occur and thus ensures compliance with strict EMC standards pursuant to applicable technical norms, see Chapter "Technical Data". Proceed as follows: 1 Mounting ferrite core Fasten a T.2400.102 ferrite core to the Dosino connection cable near to the plug.
■■■■■■■■■■■■■■■■■■■■■■ 3.14 Connecting MSB devices ■ ■ ■ Connect the connection cable of the magnetic stirrer or of the titration stand to one of the sockets marked with MSB on the rear of the control instrument. If desired, connect the rod stirrer to the stirrer socket (with stirrer symbol) of the titration stand. Start the control software. USB 1 3.14.3 Contr.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation Proceed as follows: 1 Connect a remote box ■ ■ ■ Exit the control software. Connect the remote box connection cable to one of the sockets marked with MSB on the rear of the control instrument. Start the control software. USB 1 Figure 38 Contr.
■■■■■■■■■■■■■■■■■■■■■■ 3.15 Connecting USB devices Connect a barcode reader as follows: 1 Connecting the cable ■ Plug the USB plug (Type A) of the barcode reader into one of the USB sockets on the rear side of the instrument. USB 2 USB 1 Figure 39 USB connectors 2 Configuring the barcode reader in the control software ■ Configure the barcode reader in the configuration part of the control software as described in the online Software Help.
■■■■■■■■■■■■■■■■■■■■■■ 4 Handling and maintenance 4 Handling and maintenance 4.1 General It is not only highly sensitive measuring instruments but also sample processors that require proper care. Excess contamination of the instrument may result in functional disruptions and a reduction in the service life of the sturdy mechanics and electronics of the instrument. Severe contamination can also have an influence on the measured results. Regular cleaning of exposed parts can prevent this to a large extent.
■■■■■■■■■■■■■■■■■■■■■■ 4.4 Peristaltic pump 2 Insert the filter ■ Place the filter in the tubing olive and press flat. 3 Mount the filter screw ■ 4.4 Screw the filter screw back into the tubing olive. Peristaltic pump The flow rate of the peristaltic pump depends on the drive speed, the contact pressure and, above all, the inner diameter of the pump tubing. Depending on the application, different pump tubings are used. Caution The lifetime of the pump tubings also depends on the contact pressure.
■■■■■■■■■■■■■■■■■■■■■■ 4 Handling and maintenance Selecting the pump tubing The pump tubing differs in material, diameter and hence also pumping capacity. Depending on the application, different pump tubings are used. The following table provides information on the properties and use of the pump tubing: Table 2 Pump tubing Order number Name Material Inner diameter Use 6.1826.020 Pump tubing (blue/ blue), 2-stopper PVC (Tygon ST) 1.
4.6 Quality Management and validation with Metrohm 4.6 ■■■■■■■■■■■■■■■■■■■■■■ Quality Management and validation with Metrohm Quality Management Metrohm offers you comprehensive support in implementing quality management measures for instruments and software. Further information on this can be found in the brochure «Quality Management with Metrohm» available from your local Metrohm agent. Validation Please contact your local Metrohm agent for support in validating instruments and software.
■■■■■■■■■■■■■■■■■■■■■■ 5 Troubleshooting 5 Troubleshooting 5.1 Problems and their solutions Problem Cause Remedy Marked rise in pressure Injection valve – valve blocked. Rinse the valve with water in the opposite direction or have it cleaned (by Metrohm service technician). The Swing Head either misses the rack positions totally or is inaccurate Sample Processor – The Swing Head is not correctly configured. Enter the correct values for Swing radius, Swing offset etc.
■■■■■■■■■■■■■■■■■■■■■■ 6.1 Remote interface 6 Appendix 6.1 Remote interface The 6.2148.010 remote box allows devices to be controlled which cannot be connected directly to the MSB interface of the Sample Processor. 1 2 3 Figure 41 Connectors of the remote box 1 Cable For connecting the Sample Processor. 3 Remote connector For connecting devices with a remote interface. 6.1.1 2 MSB connector Metrohm Serial Bus. For connecting external dosing devices or stirrers.
■■■■■■■■■■■■■■■■■■■■■■ 6 Appendix Inputs +5 V approx. 50 kΩ Pull-up tp tp >20 ms active = low, inactive = high The input lines can be scanned with the SCAN command. Outputs Open Collector tp tp >200 ms active = low, inactive = high IC = 20 mA, VCEO = 40 V +5 V: maximum load = 20 mA The output lines can be set with the CONTROL command. Table 3 858 Professional Sample Processor Inputs and outputs of the remote interface Assigment Pin No. Assigment Pin No.
■■■■■■■■■■■■■■■■■■■■■■ 7.1 Lift and turntable 7 Technical data 7.1 Lift and turntable Stroke path 235 mm Maximum lift load Approx. 30 N Lift rate Adjustable, 5…25 mm/s Shift rate Adjustable, 3...20 angle degrees/sec 7.2 786 Swing Head Maximum load Approx. 15 N Swing rate 10...55 angle degrees/sec Beaker sensor connector M8 socket 7.3 Two-channel peristaltic pump Pump rate 6…90 rpm, adjustable in 15 steps each in both directions of rotation Typical flow rate 0.
■■■■■■■■■■■■■■■■■■■■■■ 7.4 Injection valve Fill…Inject Positions 7.5 7 Technical data Interfaces and connectors Controller connection USB Upstream Port (9-pin Mini DIN socket) for connecting a computer to the control system of the device. MSB connectors MSB1…MSB3 Three 9-pin Mini DIN sockets for connecting dosing devices, stirrers, etc. USB connectors 1/2 Two USB Downstream Ports (Type A sockets), each 500 mA, for connecting Metrohm instruments or USB peripheral devices of other manufacturers.
■■■■■■■■■■■■■■■■■■■■■■ 7.7 Safety specifications 7.7 Safety specifications Design and testing According to EN/IEC/UL 61010-1, EN/IEC 61010-2-081, CSA-C22.2 No. 61010-1, Protection Class Ⅰ Safety instructions This document contains safety instructions which have to be followed by the user in order to ensure safe operation of the instrument. 7.
■■■■■■■■■■■■■■■■■■■■■■ 7.10 7 Technical data Reference conditions Ambient temperature 25°C (±3°C) Relative humidity ≤60% 7.11 Dimensions Width 0.28 m Height 0.73 m Depth 0.50 m Weight (without accessories) 1.858.0010: 15.50 kg 1.858.0020: 15.55 kg 1.858.0030: 15.
■■■■■■■■■■■■■■■■■■■■■■ 8.1 Declaration of Conformity 8 Conformity and warranty 8.1 Declaration of Conformity This is to certify the conformity to the standard specifications for electrical appliances and accessories, as well as to the standard specifications for security and to system validation issued by the manufacturing company.
■■■■■■■■■■■■■■■■■■■■■■ 8 Conformity and warranty EN 61010-2-081 Manufacturer Particular requirements for automatic and semiautomatic laboratory equipment for analysis and other purposes Metrohm Ltd., CH-9101 Herisau/Switzerland Metrohm Ltd. is holder of the SQS-certificate ISO 9001:2000 Quality management system for development, production and sales of instruments and accessories for ion analysis. Herisau, January 27, 2006 D. Strohm Ch.
■■■■■■■■■■■■■■■■■■■■■■ 8.3 Warranty (guarantee) Components All components used in the Metrohm instruments have to satisfy the quality standards that are defined and implemented for our products. Suppliers of components are audited by Metrohm as the need arises. Manufacture The measures put into practice in the production of our instruments guarantee a constant quality standard.
■■■■■■■■■■■■■■■■■■■■■■ 9 Accessories 9 Accessories Note Subject to change without notice. 9.1 Scope of delivery 9.1.1 858 Professional Sample Processor 2.858.0010 Qty. Order no. Description 1 1.858.0010 858 Professional Sample Processor 3 6.1608.080 Bottle / 300 mL Rinsing vessel for IC Sample Processors Material: PE Height (mm): 128 Outer diameter (mm): 68 Volume (mL): 300 2 6.1831.060 PEEK capillary 0.5 mm i.d., 1 m For inline dialysis and for Sample Changers.
■■■■■■■■■■■■■■■■■■■■■■ 9.1 Scope of delivery Qty. 1 Order no. Description 6.2064.000 Beaker retainer for Advanced IC Sample Processor Retaining plate for 838 Advanced Sample Processors. For holding 2.5 or 11 mL vials. 1 6.2151.000 Controller cable Length (m): 1 6.2621.300 Cable USB A – mini-DIN 8-pin 1.8 Tool set for Advanced IC Sample Processors Tool set consisting of open-end wrenches and hexagon keys. 1 6.2744.010 Pressure screw 5x With UNF 10/32 connection.
■■■■■■■■■■■■■■■■■■■■■■ Qty. 1 9 Accessories Order no. Description 6.2751.110 Splash protection Splash protection for Advanced IC/VA Sample Processors 1 6.2846.000 Sample needle (zirconium oxide) Sample needle for Sample Processors and Autosamplers in ion chromatography and voltammetry Material: Ceramic Outer diameter (inches): 1/8 Inner diameter (mm): 0.75 Length (mm): 151 4 T.240.0102 Ferrite cores Anti-interference adapters 2 Y.107.
■■■■■■■■■■■■■■■■■■■■■■ 9.1 Scope of delivery 9.1.2 Qty. 858 Professional Sample Processor 2.858.0020 Order no. Description 1 1.858.0020 858 Professional Sample Processor – Pump 3 6.1608.080 Bottle / 300 mL Rinsing vessel for IC Sample Processors Material: PE Height (mm): 128 Outer diameter (mm): 68 Volume (mL): 300 1 6.1803.030 PTFE capillary 0.5 mm i.d.
■■■■■■■■■■■■■■■■■■■■■■ Qty. 1 9 Accessories Order no. Description 6.1831.060 PEEK capillary 0.5 mm i.d., 1 m For inline dialysis and for Sample Changers. For IC Dialysis Unit, IC Sample Processor, Compact IC Autosampler, IC Filtration Sample Processor, IC Dialysis Sample Processor, IC Liquid Handling Dialysis Unit Material: PEEK Outer diameter (inches): 1/16 Inner diameter (mm): 0.5 Length (m): 1 1 6.1831.160 PEEK capillary 0.5 mm i.d.
■■■■■■■■■■■■■■■■■■■■■■ 9.1 Scope of delivery Qty. 1 Order no. Description 6.2621.300 Tool set for Advanced IC Sample Processors Tool set consisting of open-end wrenches and hexagon keys. 1 6.2739.000 Wrench For tightening connectors Length (mm): 1 6.2744.010 68 Pressure screw 5x With UNF 10/32 connection. For the connection of PEEK capillaries Material: PEEK Length (mm): 26 1 6.2744.034 Coupling nozzle - UNF 10/32, 2 pieces Connection pressure screw and pump tubing. 2 pieces.
■■■■■■■■■■■■■■■■■■■■■■ Qty. 1 9 Accessories Order no. Description 6.2744.070 Pressure screw short Short version. With UNF 10/32 connection. 5 pieces. For the connection of PEEK capillaries Material: PEEK Length (mm): 21 2 6.2744.160 Nozzle/UNF 10/32 coupling with security device Security device for connecting pump tubing to a nozzle. Material: PEEK 1 6.2751.110 Splash protection Splash protection for Advanced IC/VA Sample Processors 1 6.2846.
■■■■■■■■■■■■■■■■■■■■■■ 9.1 Scope of delivery Qty. 2 Order no. Description Y.107.0150 Adhesive capillary strap For fixing capillaries 1 6.2122.xxx Mains cable with line socket, type IEC 60320 C13 Power plug to customer specifications: Switzerland: 6.2122.020 (type SEV 12) Germany: 6.2122.040 (type CEE(7), VII) USA: 6.2122.070 (type NEMA/ASA) 1 9.1.3 Qty. 8.858.8002EN 858 Professional Sample Processor Manual 858 Professional Sample Processor 2.858.0030 Order no. Description 1 1.858.
■■■■■■■■■■■■■■■■■■■■■■ Qty. 1 9 Accessories Order no. Description 6.1825.210 PEEK sample loop 20 µL For injection valve, with 2 PEEK pressure screws Material: PEEK (metal-free) Outer diameter (inches): 1/16 Volume (mL): 0.02 2 6.1826.360 Pump tubing LFL (white/white), 3 stoppers For Sample Processors 1 6.1831.010 PEEK capillary 0.25 mm i.d. / 3 m For all IC components. Material: Outer diameter (inches): Inner diameter (mm): Length (m): 858 Professional Sample Processor PEEK 1/16 0.
■■■■■■■■■■■■■■■■■■■■■■ 9.1 Scope of delivery Qty. 1 Order no. Description 6.1831.060 PEEK capillary 0.5 mm i.d., 1 m For inline dialysis and for Sample Changers. For IC Dialysis Unit, IC Sample Processor, Compact IC Autosampler, IC Filtration Sample Processor, IC Dialysis Sample Processor, IC Liquid Handling Dialysis Unit Material: PEEK Outer diameter (inches): 1/16 Inner diameter (mm): 0.5 Length (m): 1 1 6.1831.160 PEEK capillary 0.5 mm i.d.
■■■■■■■■■■■■■■■■■■■■■■ Qty. 1 9 Accessories Order no. Description 6.2621.300 Tool set for Advanced IC Sample Processors Tool set consisting of open-end wrenches and hexagon keys. 1 6.2739.000 Wrench For tightening connectors Length (mm): 1 6.2744.010 68 Pressure screw 5x With UNF 10/32 connection. For the connection of PEEK capillaries Material: PEEK Length (mm): 26 1 6.2744.034 Coupling nozzle - UNF 10/32, 2 pieces Connection pressure screw and pump tubing. 2 pieces.
■■■■■■■■■■■■■■■■■■■■■■ 9.1 Scope of delivery Qty. 1 Order no. Description 6.2744.070 Pressure screw short Short version. With UNF 10/32 connection. 5 pieces. For the connection of PEEK capillaries Material: PEEK Length (mm): 21 1 6.2744.110 PEEK coupling pump tubing - inline filter Connection piece between pump tubing and inline filter Material: PEEK 2 6.2744.160 Nozzle/UNF 10/32 coupling with security device Security device for connecting pump tubing to a nozzle. Material: PEEK 1 6.2751.
■■■■■■■■■■■■■■■■■■■■■■ Qty. 1 9 Accessories Order no. Description 6.2846.000 Sample needle (zirconium oxide) Sample needle for Sample Processors and Autosamplers in ion chromatography and voltammetry Material: Ceramic Outer diameter (inches): 1/8 Inner diameter (mm): 0.75 Length (mm): 151 4 T.240.0102 Ferrite cores Anti-interference adapters 2 Y.107.0150 Adhesive capillary strap For fixing capillaries 1 6.2122.
■■■■■■■■■■■■■■■■■■■■■■ 9.2 Optional accessories 2.858.0010 9.2 Optional accessories 2.858.0010 Order no. Description 6.1835.020 PEEK sample aspiration tubing Used with IC Sample Processors, for filtration and dialysis applications Material: PEEK Outer diameter (inches): 1/8 6.1835.030 PEEK sample aspiration tubing For 813 Compact Autosampler Material: Outer diameter (inches): Inner diameter (mm): Length (mm): 6.1835.040 PEEK 1/8 0.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.1835.050 PEEK sample aspiration tube 9 Accessories For sample changers used for transferring larger sample volumes, e.g. for the determination of brighteners Material: PEEK Outer diameter (inches): 1/8 Inner diameter (mm): 1.58 Length (mm): 154 6.2041.310 Sample rack 12 x 250 mL Sample rack for 12 x 250 mL, one row Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 65 6.2041.
9.2 Optional accessories 2.858.0010 Order no. Description 6.2041.360 Sample rack for 12 x 150 mL ■■■■■■■■■■■■■■■■■■■■■■ Sample rack for 12 x 150 mL samples, one-row Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 55 6.2041.370 Sample rack 14 x 200 mL Sample rack for 14 x 200 mL samples, one-row Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 55 6.2041.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.2041.440 Sample rack 148 x 11 mL + 3 x 300 mL 9 Accessories Sample rack for 148 x 11 mL samples with 3 rinsing beakers Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 17 / 68 6.2041.450 Sample rack 56 x 11 mL + 56 x 50 mL Sample rack 56 x 11 mL + 56 x 50 mL Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 29 / 17 6.2041.
■■■■■■■■■■■■■■■■■■■■■■ 9.2 Optional accessories 2.858.0010 Order no. Description 6.2629.000 Screw nut to needle holder IC On Sample Processors 6.2714.010 Dialysis membrane (cellulose acetate) Nominal pore size : 0.2 µm. Set of 50 pieces. For inline dialysis Material: Cellulose acetate Outer diameter (mm): 47 6.2714.020 Filtration membrane 1 Nominal pore size : 0.2 µm. Set of 50 pieces. For inline filtration Material: Regenerated cellulose Outer diameter (mm): 47 6.2714.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.2743.047 Sample tubes 2.5 mL 9 Accessories 2.5 mL. 200 pieces. For IC Sample Processors Material: PP Volume (mL): 2.5 6.2743.050 Sample tubes 11 mL 2000 pieces. For IC Sample Processors and VA Autosampler Material: PP Outer diameter (mm): 16 Length (mm): 108 Volume (mL): 11 6.2743.057 Sample tubes 11 mL 200 pieces. For IC Sample Processors and VA Autosampler Material: PP Outer diameter (mm): 16 Length (mm): 108 Volume (mL): 11 6.2743.
■■■■■■■■■■■■■■■■■■■■■■ 9.2 Optional accessories 2.858.0010 Order no. Description 6.2743.077 Stopper with perforation 200 pieces. For IC Sample Processors Material: PP 6.2841.100 Rinsing Station for IC Sample Processor Rinsing station for optimally cleaning the sample needle. 6.5330.000 IC Equipment for dialysis Accessories kit for Inline Dialysis.
■■■■■■■■■■■■■■■■■■■■■■ Order no. 9 Accessories Description extensive data export functions, individually configurable report generator, control and monitoring of all system components and the chromatographic results. MagIC Net™ Compact complies with FDA regulation 21 CFR Part 11 as well as GLP. Dialogue languages: German, English, French, Spanish, Chinese, Korean, Japanese and more. 1 licence. 6.6059.222 MagIC Net™ 2.
9.3 Optional accessories 2.858.0020 9.3 ■■■■■■■■■■■■■■■■■■■■■■ Optional accessories 2.858.0020 Order no. Description 6.1826.310 Pump tubing LFL (orange/green), 3 stoppers Pump tubing for bromate determination using the triiodide method. 6.1826.320 Pump tubing LFL (orange/yellow), 3 stoppers For suppressor solutions, acceptor solution in Inline Dialysis and for Inline Ultrafiltration 6.1826.330 Pump tubing LFL (orange/white), 3 stoppers For all IC instruments with peristaltic pump.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.1826.340 Pump tubing LFL (black/black), 3 stoppers 9 Accessories For the sample solution in inline dialysis 6.1826.380 Pump tubing LFL (gray/gray), 3 stoppers For Inline Dilution 6.1826.390 Pump tubing LFL (yellow/yellow), 3 stoppers For the sample solution in Inline Ultrafiltration. 6.1835.
■■■■■■■■■■■■■■■■■■■■■■ 9.3 Optional accessories 2.858.0020 Order no. Description 6.1835.030 PEEK sample aspiration tubing For 813 Compact Autosampler Material: Outer diameter (inches): Inner diameter (mm): Length (mm): 6.1835.040 PEEK 1/8 0.75 167 PEEK sample aspiration tube For sample changers used for transferring smaller sample volumes, e.g. for the determination of suppressors Material: PEEK Outer diameter (inches): 1/8 Inner diameter (mm): 0.75 Length (mm): 154 6.1835.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.2041.310 Sample rack 12 x 250 mL 9 Accessories Sample rack for 12 x 250 mL, one row Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 65 6.2041.320 Sample rack 16 x 150 mL Sample rack for 16 x 150 mL samples, one-row Material: PVC Outer diameter (mm): 416 Hole diameter (mm): 56 6.2041.340 Sample rack 24 x 75 mL Sample rack for 24 x 75 mL samples, one-row. Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 35 6.2041.
9.3 Optional accessories 2.858.0020 Order no. Description 6.2041.380 Sample rack 14 x 235 mL ■■■■■■■■■■■■■■■■■■■■■■ Sample rack for 14 x 235 mL samples, one-row Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 58 6.2041.400 Sample rack 126 x 11 mL Sample rack for 126 x 11 mL samples, multi-row Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 16 / 65 6.2041.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.2041.450 Sample rack 56 x 11 mL + 56 x 50 mL 9 Accessories Sample rack 56 x 11 mL + 56 x 50 mL Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 29 / 17 6.2041.750 Sample rack 36 x 11 mL Sample rack for 36 x 11 mL sample tubes, one-row Material: PVC Outer diameter (mm): 270 Hole diameter (mm): 17 6.2041.
■■■■■■■■■■■■■■■■■■■■■■ 9.3 Optional accessories 2.858.0020 Order no. Description 6.2714.010 Dialysis membrane (cellulose acetate) Nominal pore size : 0.2 µm. Set of 50 pieces. For inline dialysis Material: Cellulose acetate Outer diameter (mm): 47 6.2714.020 Filtration membrane 1 Nominal pore size : 0.2 µm. Set of 50 pieces. For inline filtration Material: Regenerated cellulose Outer diameter (mm): 47 6.2714.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.2743.050 Sample tubes 11 mL 9 Accessories 2000 pieces. For IC Sample Processors and VA Autosampler Material: PP Outer diameter (mm): 16 Length (mm): 108 Volume (mL): 11 6.2743.057 Sample tubes 11 mL 200 pieces. For IC Sample Processors and VA Autosampler Material: PP Outer diameter (mm): 16 Length (mm): 108 Volume (mL): 11 6.2743.070 Stopper with perforation 2000 pieces. For IC Sample Processors Material: PP 6.2743.
■■■■■■■■■■■■■■■■■■■■■■ 9.3 Optional accessories 2.858.0020 Order no. Description 6.2841.100 Rinsing Station for IC Sample Processor Rinsing station for optimally cleaning the sample needle. 6.5330.000 IC Equipment for dialysis Accessories kit for Inline Dialysis. To be used with the 858 Professional Sample Processor and an additional 2-channel peristaltic pump. 6.5330.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.6059.222 MagIC Net™ 2.2 Professional CD: 1 Licence 9 Accessories Professional PC program for controlling intelligent Professional IC systems, Compact IC instruments and their peripherals such as different autosamplers, 800 Dosinos dosing systems, 771 Compact Interface, etc. The software permits control, data acquisition, evaluation and monitoring as well as report generation for ion chromatographic analyses.
9.4 Optional accessories 2.858.0030 9.4 ■■■■■■■■■■■■■■■■■■■■■■ Optional accessories 2.858.0030 Order no. Description 6.1826.310 Pump tubing LFL (orange/green), 3 stoppers Pump tubing for bromate determination using the triiodide method. 6.1826.320 Pump tubing LFL (orange/yellow), 3 stoppers For suppressor solutions, acceptor solution in Inline Dialysis and for Inline Ultrafiltration 6.1826.330 Pump tubing LFL (orange/white), 3 stoppers For all IC instruments with peristaltic pump.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.1826.340 Pump tubing LFL (black/black), 3 stoppers 9 Accessories For the sample solution in inline dialysis 6.1826.380 Pump tubing LFL (gray/gray), 3 stoppers For Inline Dilution 6.1826.390 Pump tubing LFL (yellow/yellow), 3 stoppers For the sample solution in Inline Ultrafiltration. 6.1835.
■■■■■■■■■■■■■■■■■■■■■■ 9.4 Optional accessories 2.858.0030 Order no. Description 6.1835.030 PEEK sample aspiration tubing For 813 Compact Autosampler Material: Outer diameter (inches): Inner diameter (mm): Length (mm): 6.1835.040 PEEK 1/8 0.75 167 PEEK sample aspiration tube For sample changers used for transferring smaller sample volumes, e.g. for the determination of suppressors Material: PEEK Outer diameter (inches): 1/8 Inner diameter (mm): 0.75 Length (mm): 154 6.1835.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.2041.310 Sample rack 12 x 250 mL 9 Accessories Sample rack for 12 x 250 mL, one row Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 65 6.2041.320 Sample rack 16 x 150 mL Sample rack for 16 x 150 mL samples, one-row Material: PVC Outer diameter (mm): 416 Hole diameter (mm): 56 6.2041.340 Sample rack 24 x 75 mL Sample rack for 24 x 75 mL samples, one-row. Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 35 6.2041.
9.4 Optional accessories 2.858.0030 Order no. Description 6.2041.380 Sample rack 14 x 235 mL ■■■■■■■■■■■■■■■■■■■■■■ Sample rack for 14 x 235 mL samples, one-row Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 58 6.2041.400 Sample rack 126 x 11 mL Sample rack for 126 x 11 mL samples, multi-row Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 16 / 65 6.2041.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.2041.450 Sample rack 56 x 11 mL + 56 x 50 mL 9 Accessories Sample rack 56 x 11 mL + 56 x 50 mL Material: PVC Outer diameter (mm): 420 Hole diameter (mm): 29 / 17 6.2041.750 Sample rack 36 x 11 mL Sample rack for 36 x 11 mL sample tubes, one-row Material: PVC Outer diameter (mm): 270 Hole diameter (mm): 17 6.2041.
■■■■■■■■■■■■■■■■■■■■■■ 9.4 Optional accessories 2.858.0030 Order no. Description 6.2714.010 Dialysis membrane (cellulose acetate) Nominal pore size : 0.2 µm. Set of 50 pieces. For inline dialysis Material: Cellulose acetate Outer diameter (mm): 47 6.2714.020 Filtration membrane 1 Nominal pore size : 0.2 µm. Set of 50 pieces. For inline filtration Material: Regenerated cellulose Outer diameter (mm): 47 6.2714.
■■■■■■■■■■■■■■■■■■■■■■ Order no. Description 6.2743.057 Sample tubes 11 mL 9 Accessories 200 pieces. For IC Sample Processors and VA Autosampler Material: PP Outer diameter (mm): 16 Length (mm): 108 Volume (mL): 11 6.2743.070 Stopper with perforation 2000 pieces. For IC Sample Processors Material: PP 6.2743.077 Stopper with perforation 200 pieces. For IC Sample Processors Material: PP 6.2841.100 Rinsing Station for IC Sample Processor Rinsing station for optimally cleaning the sample needle.
■■■■■■■■■■■■■■■■■■■■■■ 9.4 Optional accessories 2.858.0030 Order no. Description 6.5330.010 IC Equipment for ultrafiltration Accessories kit for Inline Ultrafiltration. To be used with the 858 Professional Sample Processor. 6.5330.020 IC Equipment for dilution Accessories kit for Inline Dilution.
■■■■■■■■■■■■■■■■■■■■■■ Order no. 9 Accessories Description Dosino, 771 Compact Interface, etc. The software permits control, data acquisition, evaluation and monitoring as well as report generation for ion chromatographic analyses.
■■■■■■■■■■■■■■■■■■■■■■ Index Index Numbers/Symbols 685 Dosimat ............................ 36 700 Dosino .............................. 36 741 Stirrer ................................ 28 772 Pump Unit ......................... 29 800 Dosino .............................. 36 801 Stirrer ................................ 37 802 Stirrer ................................ 28 803 Ti Stand ............................. 37 804 Ti Stand ............................. 37 805 Dosimat ............................
■■■■■■■■■■■■■■■■■■■■■■ Index W Warranty ..................................