User Manual

4.6 Standard methods
766 IC Sample Processor
81
Settings in the «IC Metrodata» program
Definition of IC method (analysis time, start parameters for IC instru-
ments 732, 733 and 709, etc.), additional association of this method
with the following time program for the 732 IC Detector:
Method / Equipment / Setup / Program / Text:
0.0 Puls_766_set Set remote line 3 at 732/1 to 1 (s. below)
0.1 Puls_766_reset Set remote line 3 at 732/1 to 0 (s. below)
0.2 Flag end Program end
Method / Equipment / Setup / Program / Remote configuration:
Puls_766_set = **1***** Set remote line 3 at 732/1 to 1
Puls_766_reset = **0***** Set remote line 3 at 732/1 to 0
Method / Equipment:
Start with method
Procedure at program start
1. Start 766 IC Sample Processor with <START>.
2. Create new queue in the program «IC Metrodata» and start it.
4.6.3 Method "SP"
Application
Processing a queue with the PC program «IC Metrodata» with the 766
IC Sample Processor as "Master".
Interconnection
see Fig. 11 (without suppression) and Fig. 12 (with suppression)
Program of 766 IC Sample Processor
766 IC Sample Proc. 11111 5.766.0010
parameters
method SP
number of samples: rack
>start sequence
1 CTL:Rm: INIT
2 CTL:Rm: PUMP 752 ON
>sample sequence
1 SCN:Rm : Pump1 ?
2 MOVE 1 : sample
3 LIFT: 1 : work mm
4 CTL:Rm: FILL A 1
5 PUMP 1.1 : 120 s
6 CTL:Rm: ZERO 1
7 CTL:Rm: INJECT A 1
8 WAIT 1200 s
>final sequence
1 CTL:Rm: PUMP R/S 1
2 CTL:Rm: PUMP 752 OFF
>changer settings
rack number 0
lift rate 1 12 mm/s
shift rate 20
>manual stop
CTL Rmt: **************
CTL RS232:
------------
− Report header with serial number and program ver-
sion
− Method name
− Number of samples to be processed (entire sample
rack)
− Initialize remote interface
− Switch on 752 Pump Unit for suppressor
− Waiting until 709 IC Pump runs
− Move needle to sample
− Place lift with needle to working position
− Switch injection valve A at 733 to "Fill"
− Fill sample loop with sample during 120 s
− Trigger autozero at 732 IC Detector
− Switch injection valve A at 733 to "Inject"
− Waiting time for recording and evaluation of the
chromatogram (must be adapted)
− Switch off 709 IC Pump
− Switch off 752 Pump Unit
− —— Settings for changer functions ——
− —— Reaction to manual stop ———