Owner manual
5.7.3 Alphabetical instruction list
746 VA Trace Analyzer / 747 VA Stand
5-291
SMPL>M Page: O, S Stand: M, A Abbreviation: SMPL>
Instructions t/s Main parameters Auxiliary parameters
––––––––––––– ––––– ––––––––––––––––––––––––– –––––––––––––––––––––––––
## .. SMPL>M ..... V.fraction ........mL V.total .........L
Function Add sample volume to the measuring vessel (MEAS).
Parameter Range; Default value / Meaning
V.fraction 0.010...50.000 mL; -
Fractional volume
With diluted samples, here the volume fraction of the total volume
V.total which is added to the sample vessel must be entered. The
following condition holds:
V.fraction ≤≤ V.total
V.total 0.10 mL...100000 L; -
Total volume
With diluted samples, here the total volume of sample and dilution
solution must be entered. The following condition holds:
V.total ≥≥ V.fraction
Description The SMPL>M instruction is used for the manual or automatic addition of
the sample volume to the measuring vessel (MEAS) on the 747 VA
Stand:
− In manual addition or addition with the 6.5611.010 Pipet-
ting equipment, the prompt SMPL "V.sample" > M for
manual addition of the sample volume V.sample appears
in the program run.
− In automatic addition with the 695 Autosampler, the sam-
ple volume is transferred from the sample vessel on the
sample rack defined on the 1
st
sample data line to the
measuring vessel.
With undiluted samples (V.fraction and V.total blank), the sample
volume is given either by S0 (on entry of S0 as a volume) or by S0/S2
(on entry of S0 as a weight, S2 is the density in g/mL).
With diluted samples (V.fraction > 0 and V.total ≥≥ V.fraction), the
sample volume is given by V.fraction, irrespective of the entry of S0.
You will find further details on the sample size in the description of the
parameter Sample size/S0 in section 5.4.4.
see also SMPL/M, SMPL/F