Owner's manual
Table Of Contents
- Table of contents
- Table of figures
- 1 Introduction
- 2 Overview of the instrument
- 3 Installation
- 4 Operation
- 4.1 Fundamentals of operation
- 4.2 Instrument and Program Settings
- 4.3 Program information
- 4.4 Calibration functions
- 4.5 Methods
- 4.6 Determinations
- 4.6.1 Preparing samples
- 4.6.2 Preparing the instrument and the accessories
- 4.6.3 Preparing the determination
- 4.6.4 Starting the determination
- 4.6.5 Cleaning the instrument and accessories
- 4.6.6 Adjusting the method parameters during the determination
- 4.6.7 Stopping the determination manually
- 4.6.8 Status of the live curve
- 4.7 Results
- 4.8 GLP functions
- 5 Handling and maintenance
- 6 Troubleshooting
- 7 Technical specifications
- 8 Conformity and warranty
- 9 Accessories
- Index
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Table of contents
743 Rancimat
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III
Table of contents
1 Introduction 1
1.1 Instrument description ......................................................... 1
1.2 Rancimat method ................................................................. 2
1.3 About the documentation ................................................... 3
1.3.1 Symbols and conventions ........................................................ 3
1.4 Safety instructions ................................................................ 4
1.4.1 General notes on safety ........................................................... 4
1.4.2 Electrical safety ........................................................................ 5
1.4.3 Flammable solvents and chemicals ........................................... 6
1.4.4 Recycling and disposal ............................................................. 6
2 Overview of the instrument 7
3 Installation 10
3.1 Setting up the instrument .................................................. 10
3.1.1 Packaging .............................................................................. 10
3.1.2 Checks .................................................................................. 10
3.1.3 Location ................................................................................ 10
3.2 Mounting accessories ......................................................... 10
3.2.1 Mounting accessories for the internal air supply ..................... 10
3.2.2 Mounting accessories for the external air supply .................... 13
3.2.3 Equipping the reaction and measuring vessels ........................ 13
3.2.4 Inserting vessels / Establishing tubing connections ................. 16
3.2.5 Mounting the exhaust collection tube (optional accessories) .. 17
3.3 Mains connection ............................................................... 18
3.3.1 Checking the mains voltage ................................................... 18
3.3.2 Replacing fuses ...................................................................... 18
3.3.3 Mains cable and mains connection ........................................ 19
3.3.4 Switching the instrument on/off ............................................ 19
3.4 Connecting a PC ................................................................. 19
3.4.1 Connecting the 743 Rancimat and the PC .............................. 19
3.4.2 Installing the software ........................................................... 20
3.4.3 Carrying out basic settings ..................................................... 22
4 Operation 24
4.1 Fundamentals of operation ............................................... 24
4.1.1 Starting and exiting the program ........................................... 24
4.1.2 Terms .................................................................................... 25
4.1.3 Control window .................................................................... 25
4.1.4 Results window ..................................................................... 27
4.1.5 File types ............................................................................... 30
4.1.6 Context-sensitive menus ........................................................ 31