User guide

Table of contents
732 IC Detector / 733 IC Separation Center
I
Table of contents
1 Introduction............................................................................................1
1.1 Instrument description.............................................................................1
1.2 Parts and controls.....................................................................................3
1.2.1 732 IC Detector .............................................................................3
1.2.2 733 IC Separation Center.............................................................. 5
1.3 Information on the Instructions for Use................................................8
1.3.1 Organization ..................................................................................8
1.3.2 Notation and pictograms............................................................... 9
1.4 Safety notes .............................................................................................10
1.4.1 Electrical safety............................................................................10
1.4.2 General precautionary rules........................................................10
2 Installation...........................................................................................11
2.1 Flow chart.................................................................................................11
2.2 Setting up the instruments....................................................................12
2.2.1 Packaging....................................................................................12
2.2.2 Check ..........................................................................................12
2.2.3 Location....................................................................................... 12
2.2.4 Arrangement of the instruments.................................................. 12
2.3 Connection of 733 IC Separation Center.............................................13
2.3.1 733.0010/733.0X30 IC Separation Center................................... 13
2.3.2 733.0X20 IC Separation Center...................................................14
2.3.3 Connection of syringe and suction tubing..................................16
2.3.4 Connection of the drain tube....................................................... 16
2.3.5 Connection of the 6.5324.000 Bottle rack (option) ..................... 16
2.4 Mains connection....................................................................................17
2.4.1 Setting the mains voltage............................................................17
2.4.2 Fuses...........................................................................................18
2.4.3 Mains cable and mains connection ............................................ 18
2.4.4 On/off switching of the instruments ............................................18
2.5 Capillary connections.............................................................................19
2.5.1 Capillaries....................................................................................19
2.5.2 Steel connectors.......................................................................... 19
2.5.3 PEEK connectors ........................................................................20
2.6 Connection of 709 IC Pump...................................................................21
2.6.1 Electrical connection ...................................................................21
2.6.2 Pulsation dampener .................................................................... 21
2.6.3 Filter unit PEEK............................................................................22
2.6.4 Filter unit Manufit .........................................................................23
2.6.5 Connection to injection valve with PEEK capillaries ...................24
2.6.6 Connection to injection valve with steel capillaries.....................25
2.6.7 Passivation of the IC system.......................................................27
2.7 Precolumns..............................................................................................28
2.7.1 General information on precolumns............................................28
2.7.2 Precolumns with twin cartridge holder........................................28
2.7.3 Precolumns with cartridge head .................................................30
2.7.4 IC anion precolumn SUPERSEP .................................................31