Original instructions User’s Manual CentriVap® Complete™ Models 73150 Series To receive important product updates, complete your product registration card online at register.labconco.com Labconco Corporation 8811 Prospect Avenue Kansas City, MO 64132-2696 800-821-5525, 816-333-8811 Fax 816-363-0130 E-MAIL labconco@labconco.com HOME PAGE www.labconco.com Please read the User’s Manual before operating the equipment.
Original instructions Copyright © 2012, 2013 Labconco Corporation. All rights reserved. The information contained in this manual and the accompanying products are copyrighted and all rights reserved by Labconco Corporation. Labconco Corporation reserves the right to make periodic design changes without obligation to notify any person or entity of such change. Warranty Labconco provides a warranty on all parts and factory workmanship.
Original instructions TABLE OF CONTENTS CHAPTER 1: INTRODUCTION Safety Symbols 1 2 CHAPTER 2: PREREQUISITES Electrical Requirements Location and Exhaust Requirements Space Requirements 3 3 4 4 CHAPTER 3: GETTING STARTED Unpacking Your CentriVap CentriVap Components Setting Up Your CentriVap Emergency Access Into the Chamber Exhaust Port Electrical Connection Rotor Installation Chemical Resistance of CentriVap Components Solvent Safety Precautions 5 6 6 7 7 8 8 8 8 9 CHAPTER 4: USING YOUR CENTRIVAP CO
Original instructions CHAPTER 5: MAINTAINING YOUR CENTRIVAP COMPLETE 18 CHAPTER 6: ACCESSORIES FOR YOUR CENTRIVAP COMPLETE Installing a Vacuum Gauge Installing a Secondary Chemical Trap 20 22 23 CHAPTER 7: TROUBLESHOOTING 24 APPENDIX A: CENTRIVAP COMPONENTS 27 APPENDIX B: CENTRIVAP DIMENSIONS 29 APPENDIX C: CENTRIVAP SPECIFICATIONS Electrical Specifications Environmental Conditions Evaporation Rates 30 30 31 32 DECLARATION OF CONFORMITY 34
Original instructions Chapter 1: Introduction Congratulations on your purchase of a Labconco CentriVap Complete. Models are available for operation on 115V or 230V. The CentriVap Complete combines a concentrator, cold trap, and vacuum pump in one cabinet. The concentrator uses centrifugal force with heat and vacuum to rapidly evaporate and condense solvents from biological and analytical samples.
Original instructions Chapter 1: Introduction Safety Symbols Your CentriVap Complete was designed with safety in mind, however conditions may exist that could be hazardous. Throughout this manual potentially hazardous conditions are identified using the following words and symbols. It is important that you understand the warnings listed throughout this manual before you operate the CentriVap Complete.
Original instructions Chapter 2: Prerequisites Before you install your CentriVap, you need to prepare your site for installation. Carefully examine the location where you intend to install your CentriVap. You must be certain that the area is level and of solid construction. In addition, an exhaust means must be provided. An electrical source must be located near the installation site. Carefully read this chapter to learn: • The electrical supply requirements. • The exhaust requirements.
Original instructions Chapter 2: Prerequisites ! Do not position the CentriVap so that it is difficult to remove the power cord from the unit or to operate the power switch. Do not use any detachable power cord that is not adequately rated for the unit. Location and Exhaust Requirements The CentriVap Complete should be located on a surface that is stable, flat and level. WARNING: The CentriVap should be located within a fume hood if hazardous or flammable solvents are used.
Original instructions Chapter 3: Getting Started Now that the site for your CentriVap Complete is properly prepared, you are ready to unpack, inspect, install, and test your CentriVap Complete. Read this chapter to learn how to: • Unpack and move your CentriVap Complete. • Set up your CentriVap Complete. • Connect the electrical supply source to your CentriVap Complete. • Properly exhaust your CentriVap Complete. • Safely use solvents with your CentriVap Complete.
Original instructions Chapter 3: Getting Started Unpacking Your CentriVap Carefully unpack your CentriVap and inspect it for damage that may have occurred in transit. If your CentriVap is damaged, notify the delivery carrier immediately and retain the entire shipment intact for inspection by the carrier. The United States Interstate Commerce Commission rules require that claims be filed with the delivery carrier within fifteen (15) days of delivery.
Original instructions Chapter 3: Getting Started Plus the following: Part # 7314000 7396206 7455100 7455101 7450200 Component Description User’s Manual Coupling Insert Rotor, 12-13 mm (Standard Models) Rotor, 12-13 mm PTFE (Acid Resistant Models) Glass Jar If you do not receive one or more of the components listed for your CentriVap, or if any of the components are damaged, contact Labconco Corporation immediately for further instructions.
Original instructions Chapter 3: Getting Started Exhaust Port If the CentriVap is not located in a fume hood, attach one end of a user-supplied 3/8" ID hose to the exhaust port on the back of the unit. Clamp securely. Route the other end to a fume hood or other laboratory ventilation device. Electrical Connection Plug the power cord into the receptacle on the back of the CentriVap Concentrator and plug the other end into a suitable power receptacle.
Original instructions Chapter 3: Getting Started When using compounds in the CentriVap that are hostile to the materials of construction, it is imperative that the equipment is appropriately maintained. • After each run, clean up all residues, spills and materials that might have splashed in the chamber using agents suitable for the substance involved. • Drain the cold trap immediately after the collected ice is melted to prevent corrosive liquids from residing in the trap.
Original instructions Chapter 3: Getting Started Do not store flammable or hazardous solvents within 12 inches (300 mm) of the CentriVap. IMPORTANT: Various Federal, State or local regulations may govern the disposal of substances used in connection with this equipment. All users of this equipment are urged to become familiar with any regulations that apply in the user’s area concerning the dumping of waste materials in or upon water, land or air and to comply with such regulations.
Original instructions Chapter 4: Using Your CentriVap Complete After your CentriVap Complete has been installed as detailed in Chapter 3: Getting Started, you are ready to begin using your CentriVap. Read this chapter to learn how to: • Set operating parameters. • Operate the controls. • Properly select and position glassware inside your CentriVap. • Understand the display. • Interrupt a cycle after it has begun. NOTE: See Appendix C: CentriVap Specifications for electrical requirements.
Original instructions Chapter 4: Using Your CentriVap Complete Planning Thoroughly understand procedures and the equipment operation prior to beginning work. The unique performance of the CentriVap is dependent upon the proper balance of heat, vacuum and centrifugal force. If the proper balance is not established, it is possible to damage or lose a portion of the sample.
Original instructions Chapter 4: Using Your CentriVap Complete The tables in Appendix C: CentriVap Specifications indicate approximate times required to evaporate various common solvents. Actual times must be determined by the user. The CentriVap can be set to alarm after a preset period of operation. When the time expires, the CentriVap will give an audible alarm and turn itself off.
Original instructions Chapter 4: Using Your CentriVap Complete 7. Set Point Select Button – To select a parameter to change, press the select button. Arrows on the display will point to the parameter that may be altered. 8. Heat Boost Button – If the model is so equipped, pressing the button will activate or deactivate the auxiliary Heat Boost heater. 9. Cold Trap Button – Used to start or stop the refrigeration system for the cold trap.
Original instructions Chapter 4: Using Your CentriVap Complete If during a run the “STOP” button is pressed, the timers remember the time at which stop occurred. If “RUN” is then pressed, the timers continue to count down from the time at which they were stopped. If you are running program 1, program 2 or program 3, pressing “PROG 1,” “PROG 2” or “PROG 3” resets the timers to the original set point time and the CentriVap starts a new run.
Original instructions Chapter 4: Using Your CentriVap Complete 9. Press “RUN.” If the display was showing set point parameters, it will change to show actual parameters. Press “RUN” again. The “S” (STOP) in the display changes to “R” (RUN). The program on the display alternately displays “R” or the number of the program that is running. If you intend to run program 1, 2 or 3, simply press “PROG 1,” “PROG 2” or “PROG 3” to quick start the CentriVap.
Original instructions Chapter 4: Using Your CentriVap Complete Interrupting a Cycle After it Has Begun At any time during a run, the cycle may be stopped by pressing the “STOP” button. This shuts off all operating functions. After the rotor stops, the lid may be opened. If it is necessary to re-start the CentriVap, close the lid and press “RUN.” The CentriVap resumes operation at the same set point parameters and the timer continues to count down from the time at which the CentriVap was stopped.
Original instructions Chapter 5: Maintaining Your CentriVap Complete Under normal operation, the CentriVap Complete requires little maintenance. The following maintenance schedule is recommended. Before servicing the CentriVap, disconnect electrical power. Special precautions must be observed if materials used in the CentriVap are known to be hazardous, toxic, radioactive or contaminated with pathogenic micro organisms. Before servicing, the CentriVap must be suitably decontaminated.
Original instructions Chapter 5: Maintaining Your CentriVap Complete 8. Check continuity of the protective earth between the ground terminal on the power inlet and a bare metal housing panel. Contact Labconco if there is no continuity. 9. Repair any defects to the surface where the CentriVap is installed. Monthly: 1. The rubber components on the CentriVap may eventually deteriorate and require replacement. The effective life of rubber parts depends upon both their usage and the surrounding environment.
Original instructions Chapter 6: Accessories for Your CentriVap Complete The configuration of your CentriVap Complete can be changed to accommodate your needs. Read this chapter to learn how to: 20 • Install a vacuum gauge. • Install a secondary chemical trap.
Original instructions Chapter 6: Accessories for Your CentriVap Complete The following accessories are available for the CentriVap Complete. PART # 7462900 7462901* 7450700 7450701* 7455000 7455001* 7455100 7455101* 7455200 7455201* 7553100 7553101* 7553000 7553001* DESCRIPTION Rotor (DNA) Holds (72) 0.5 ml microcentrifuge tubes and (60) 1.5 ml microcentrifuge tubes or (60) 2.0 ml microcentrifuge tubes Rotor (1.5 ml) Holds (132) 1.5 ml microcentrifuge tubes or (132) 2.
Original instructions Chapter 6: Accessories for Your CentriVap Complete PART # DESCRIPTION 7461900 7461901* Rotor (96 well plate) Holds (4) Standard 96 well plates or (2) Deep well 96 well plates Clear Canister – Accommodates inserts listed below Acid Trap Insert Moisture Trap Insert Ammonia Trap Insert Radiochemical Trap Insert Solvent Trap Insert 7460900 7814800 7814900 7995600 7815000 7815200 Installing a Vacuum Gauge A user-supplied vacuum gauge may be attached to the CentriVap to monitor the vac
Original instructions Chapter 6: Accessories for Your CentriVap Complete Installing a Secondary Chemical Trap An accessory secondary chemical trap is available to minimize the exhausting of solvents into the atmosphere. Attach the bracket to the right hand side of the housing using the screws provided. Attach the hose from the outlet on the vacuum pump to the “out” connector of the canister housing. Unscrew the clear blow of the canister housing from the head.
Original instructions Chapter 7: Troubleshooting Refer to the following if your CentriVap fails to operate properly. If the suggested corrective actions do not solve your problem, contact Labconco for additional assistance. The following failure codes may appear on the display when problems are sensed by the internal self check routine. CAUTION: Disconnect power before corrective action is taken. DISPLAY ERROR CODE CAUSE CORRECTIVE ACTION Heat Sensor Sensor failure Replace sensor assembly.
Original instructions Chapter 7: Troubleshooting Other corrective actions for potential problems are as follows: PROBLEM Unit will not operate CAUSE CORRECTIVE ACTION Unit not connected to electrical power Connect unit to proper electrical receptacle. Circuit breaker blown Correct electrical problem and reset circuit breaker by pressing button. Lid open Close lid. Excessive vibration Sample tubes not located symmetrically in rotor Reposition sample tubes.
Original instructions Chapter 7: Troubleshooting PROBLEM Recovery of condensate in Cold Trap is less than normally expected CAUSE Cold Trap is not ON CORRECTIVE ACTION Check to make sure switch is ON and condensing unit fan is moving air out of the sides of the cabinet. Cold Trap does not cool down Turn vacuum pump OFF and allow Cold Trap to cool for at least 30 min. to reach temperature. -50°C temperature can be checked with a solvent thermometer or digital thermometer.
Original instructions Appendix A: CentriVap Components The following pages list components that are available for your CentriVap Complete. The parts shown are the most common replacement parts. If other parts are required, contact Product Service.
Original instructions Appendix A: CentriVap Components 28 Product Service 1-800-522-7658
Original instructions Appendix B: CentriVap Dimensions Product Service 1-800-522-7658 29
Original instructions Appendix C CentriVap Specifications This Appendix contains technical information about the CentriVap including specifications, environmental operating conditions and evaporation rates. Mechanical Specifications • Weight: 145 lbs. (66 kg) • Dimensions: See Appendix B Electrical Specifications 30 • Nominal amperage for 115V/60 Hz CentriVap: 12A. • Nominal amperage for 230V/50Hz CentriVap: 6.5A. • Nominal amperage for 230V/60Hz CentriVap: 6.5A.
Original instructions Appendix C: CentriVap Specifications Environmental Conditions • Indoor use only. • Maximum altitude: 6562 feet (2000 meters). • Ambient temperature range: 41° to 104°F (5° to 40°C). • Maximum relative humidity: 80% for temperatures up to 88°F (31°C), decreasing linearly to 50% relative humidity at 104°F (40°C). • Main supply voltage fluctuations not to exceed ±10% of the nominal voltage.
Original instructions Appendix C: CentriVap Specifications Evaporation Rates Methylene Chloride bp 40 Tube Size (ml) Number of Samples Sample Size (ml) Heater Temp (C) Heat Boost Vacuum Pump Time to Dry (min) Cold Trap Rate Overall (ml/min) 50 50 15 15 12 12 18 18 25 25 10 10 45 45 45 45 off on off on Diaphragm Diaphragm Diaphragm Diaphragm 93 89 57 55 yes yes yes yes 3.23 3.37 3.16 3.
Original instructions Appendix C: CentriVap Specifications bp 100 Water Tube Size (ml) Number of Samples Sample Size (ml) Heater Temp (C) Heat Boost Vacuum Pump Time to Dry (min) Cold Trap Rate Overall (ml/min) 50 50 50 15 1.5 1.5 1.5 1.5 1.
Original instructions 34 Product Service 1-800-522-7658
