Instruction Manual HI 9932 Autoranging Bench Microprocessor EC/TDS/NaCl/°C Meter Manufacturers since 1978 This Instrument is in Compliance with the CE Directives
Dear Customer, Thank you for choosing a Hanna Instruments Product. Please read this instruction manual carefully before using the instrument. This manual will provide you with the necessary information for a correct use of the instrument, as well as a precise idea of its versatility. If you need additional technical information, do not hesitate to e-mail us at tech@hannainst.com. These instruments are in compliance with directives. TABLE OF CONTENTS PRELIMINARY EXAMINATION .................................
PRELIMINARY EXAMINATION Remove the instrument from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any damage, notify your Dealer. Each meter is supplied complete with: • HI 76310 Conductivity/TDS probe • 12V DC power adapter • Dust Cover. Note: Save all packing material until you are sure that the instrument functions correctly. Any defective item must be returned in its original packaging together with the supplied accessories.
FUNCTIONAL DESCRIPTION 1) 2) 3) 4) Liquid Crystal Display (LCD) ALT key, to alternate key function CAL / CALT key, to enter calibration mode RANGE / FIXED key, to select measurement range or (with ALT) to freeze the current range on the LCD 5) ATC / TC key, to select temperature compensation mode or (with ALT) to view the temperature coefficient value 6) GLP key, to display GLP data 7) WCFM key, to move down or (with ALT) confirm values 8) VFNC key, to move up or (with ALT) enter setup mode 9) ON/OFF key,
SPECIFICATIONS Range EC 0.00 to 29.99 µS/cm (Autoranging) 30.0 to 299.9 µS/cm 300 to 2999 µS/cm 3.00 to 29.99 mS/cm 30.0 to 200.0 mS/cm Up to 500.0 mS/cm actual(*) Conductivity TDS 0.00 to 14.99 ppm (Autoranging) 15.0 to 149.9 ppm 150 to 1499 ppm 1.50 to 14.99 g/L 15.0 to 100.0 g/L Up to 400.0 g/L actual(*) TDS (with 0.80 factor) NaCl 0.0 to 400.0 % Temp. 0.0 to 60.0 C Resolution EC 0.01 µS/cm (from 0.00 to 29.99 µS/cm) 0.1 µS/cm (from 30.0 to 299.9 µS/cm) 1 µS/cm (from 300 to 2999 µS/cm) 0.
EC Calibration NaCl Calibration Temperature Calibration Temperature Compensation Temperature Coefficient TDS Factor Probe GLP Serial Interface Auto Off Power supply Casing Environment Dimensions Weight 1 point with 6 memorized buffers 84,1413,5000,12880,80000,111800 µS/cm 1 point with HI 7037 buffer (optional) 2 points at 0 and 50 C (plus ±1 C adjustment) Automatic or Manual from 0 to 60 C (can be disabled to measure actual conductivity) 0.00 to 6.00 %/ C (for EC and TDS only) Default value is 1.90%/ C 0.
TAKING MEASUREMENTS Press the ON/OFF key to turn the meter on. Immerse the probe into the solution to be tested. The sleeve holes must be completely submerged. Tap the probe repeatedly to remove any air bubbles that may be trapped inside the sleeve. If needed, press the RANGE key repeatedly until the desired range (EC, TDS, NaCl) is selected on the LCD. Allow for the reading to stabilize. The upper LCD displays the measure in the selected range while the temperature is displayed on the lower LCD.
AUTORANGING The EC and TDS scales are autoranging. The meter automatically sets the scale with the highest possible resolution. By pressing ALT+FIXED, the autoranging feature is disabled and the current range is frozen on the LCD. "F1" symbol blinks on the LCD. To restore the autoranging option press ALT+FIXED again. Note: Autoranging is automatically restored if the range is changed, if the setup or calibration modes are entered and if the meter is turned off and back on again.
EC/TDS/M Ω CALIBRATION EC/TDS/MΩ Calibration is a 1-point procedure. Selectable calibration points are: 0.0, 84.0µS, 1413µS, 5.00mS, 12.88mS, 80.0mS,111.8mS. To enter EC calibration select the EC range and press the CAL key. Note: TDS reading is automatically derived from the EC reading and no specific calibration for TDS is needed. Pressing CAL while TDS range is selected has no effect. Rinse the probe with some of the calibration solution or deionized water. Immerse the probe into the solution.
III IV V In order to minimize any EMC interference, use plastic beakers. The meter uses 1.90%/ C compensation factor during calibration. If the setup item "tc" has been set to a different value, when exiting the calibration mode the value displayed on the upper LCD could be different from the nominal buffer value. It is possible to set the cell constant value directly without following the calibration procedure. To set the cell constant enter the setup mode and select "CEL" (see SETUP for details).
TEMPERATURE CALIBRATION (for technical personnel only) The calibration is 2 points at 0.0, 50.0 C. • Immerse the probe in a 0 C temperature bath. • Press ALT+CALT to enter temperature calibration mode. • The lower LCD displays "0.0 C"; "BUF" and "CAL" tags appear. • When the reading is stable, "CON" symbol starts to blink. • Press ALT+CFM to confirm. The lower LCD displays 50.0 C. • Immerse the probe in a 50 C temperature bath. • When the reading is stable, "CON" symbol starts to blink.
CONDUCTIVITY VERSUS TEMPERATURE CHART The conductivity of an aqueous solution is the measure of its ability to carry an electrical current by means of ionic motion. The conductivity invariably increases with increasing temperature. It is affected by the type and number of ions in the solution and by the viscosity of the solution itself. Both parameters are temperature dependent.
SETUP Setup is used to view or change the instrument parameters. To enter setup press ALT+FNC when the meter is in measurement mode. "Set" is displayed on the upper LCD. The lower LCD displays the blinking code of the current setup item. Select the desired setup item using the V or W key. Press ALT+CFM to confirm. Note: If ALT+FNC are pressed before item confirmation, the meter will escape and return to measurement mode.
The following table lists the setup items, their valid range of values and the factory settings (default): Item Description Valid values Default tc Temp. compensation coeff. 0.00 to 6.00 %/ C 1.90 tcE Temp. compensation mode Atc, Mtc, notc Atc tdS TDS factor 0.40 to 0.80 0.50 CEL Cell constant (K) 0.500 to 1.700 1.000 AoF Auto-Off enabled On, OFF OFF YEA Year 1999 to 2098 1999 dAt Date (DD.MM) 01.01 to 31.12 01.01 hou Time (hh.mm) 00.00 to 23.59 00.
Last calibration year. Last calibration time. Cell constant value (K). Offset value. This information is displayed only if the last calibration was performed at 0.00 µS. Calibration solution used. If the cell constant was changed after calibration (through "CEL" setup function), this information is not displayed.
DATA TRANSFER TO PC Connect the meter to a PC through the RS232 output (#11 on page 4). Use HI 920010 (9 to 9-pin) connection cable. The meter must be in measurement mode to communicate. The meter RS232 port is optoisolated and transmits data with a Baud rate of 2400 bps. Retrieve the GLP data and request the meter parameters and the current reading (of the current range only) from the PC directly. It is also possible to send a command from the PC to set the meter in a different range.
ACCESSORIES CONDUCTIVITY BUFFER SOLUTIONS HI 70030P HI 7030L HI 7030M HI 70031P HI 7031L HI 7031M HI 70033P HI 7033L HI 7033M HI 7034L HI 7034M HI 7035L HI 7035M HI 70039P HI 7039L HI 7039M HI 8030L HI 8031L HI 8033L HI 8034L HI 8035L HI 8039L HI 7037L 12880 µS/cm (µmho/cm), 20mL sachets (25 pcs.) 12880 µS/cm (µmho/cm), 460mL bottle 12880 µS/cm (µmho/cm), 230mL bottle 1413 µS/cm (µmho/cm), 20mL sachets (25 pcs.
WARRANTY All Hanna Instruments meters are warranted for two years against defects in workmanship and materials when used for their intended purpose and maintained according to instructions. The electrodes and the probes are warranted for a period of six months. This warranty is limited to repair or replacement free of charge. Damages due to accident, misuse, tampering or lack of prescribed maintenance are not covered. If service is required, contact the dealer from whom you purchased the instrument.
CE DECLARATION OF CONFORMITY Recommendations for Users Before using this product, make sure that it is entirely suitable for the environment in which it is used. Operation of this instrument in residential area could cause unacceptable interference to radio and TV equipment, requiring the operator to take all necessary steps to correct interference. The metal bands of the probe are sensitive to electrostatic discharges. Avoid touching these metal bands at all times.
HANNA LITERATURE Hanna publishes a wide range of catalogs and handbooks for an equally wide range of applications. The reference literature currently covers areas such as: • • • • • • • Water Treatment Process Swimming Pools Agriculture Food Laboratory Thermometry and many others. New reference material is constantly being added to the library. For these and others catalogs, handbooks and leaflets, contact your dealer or the Hanna Customer Service Center nearest to you.