User Manual

30 31
CALCIUM
SPECIFICATIONS
Range 0 to 400 mg/L
Resolution 10 mg/L
Accuracy ±10 mg/L ±5% of reading at 25 °C
Light Source Tungsten lamp with narrow band interference filter @ 466 nm
Method Adaptation of the Oxalate method.
REQUIRED REAGENTS
Code Description Quantity
- Buffer Reagent 4 drops
HI 93752A-0 Ca Calcium Buffer Reagent 7 mL
HI 93752B-0 Ca Calcium Oxalate Reagent 1 mL
REAGENT SETS
HI 937521-01 Reagents for 50 tests
HI 937521-03 Reagents for 150 tests
For other accessories see page 128.
MEASUREMENT PROCEDURE
Note: for sample preparation follow the COLORED OR TURBID SAMPLES procedure at page 17.
Select the
Calcium
method using the procedure described in the
Method Selection
section (see page 12).
Using the 5 mL syringe add exactly 3.00 mL of sample to the cuvette.
Use the pipette to fill the cuvette up to the
10 mL mark with the HI 93752A-0 Calcium
Buffer Reagent.
Add 4 drops of Buffer Reagent.
Calcium
Remove the cuvette and add the content of one packet of
HI 93716-0 DPD reagent. Replace the cap and shake gently for
about 20 seconds to dissolve most of the reagent.
Reinsert the cuvette into the instrument.
Press Timer and the display will show the countdown prior to the measurement or, alternatively, wait
for 2 minutes and 30 seconds and press Read. When the timer ends the meter will perform the
reading.
The instrument displays the results in mg/L of bromine.
INTERFERENCES
Interference may be caused by: Chlorine, Iodine, Ozone, Oxidized forms of Chromium and Manganese.
In case of water with hardness greater than 500 mg/L CaCO
3
, shake the sample for approximately
2 minutes after adding the reagent.
In case of water with alkalinity greater than 250 mg/L CaCO
3
or acidity greater than 150 mg/L CaCO
3
,
the color of the sample may develop only partially, or may rapidly fade. To resolve this, neutralize the
sample with diluted HCl or NaOH.
Bromine
3 mL of sample