ROSEMOUNT ANALYTICAL NGA2000 TRACE OXYGEN ANALYZER MODULE 748420-A
NOTICE The information contained in this document is subject to change without notice. This manual is based on the production version of the Trace Oxygen Analyzer Module. Hardware and/or software changes may have occurred since this printing. Rosemount Analytical's NGA 2000 system of Modular Gas Analyzers and Controllers are patented, under U.S. Patent 5.787.015. ® Teflon is a registered trademark of E.I. duPont de Nemours and Co., Inc. ® SNOOP is a registered trademark of NUPRO Co.
CONTENTS PREFACE Purpose/Safety Summary.................................................................................P1 Glossary ....................................................................................................P3 Specifications - General...................................................................................P5 Specifications - Sample ....................................................................................P5 Specifications - Physical ...........................
CONTENTS SECTION 2. INSTALLATION 2.1 Unpacking ................................................................................................. 5 2.2 Assembly................................................................................................... 5 2.2.1 Electrolyte Addition ........................................................................ 5 2.3 Location .................................................................................................... 6 2.4 Gases .....................
CONTENTS SECTION 4. MAINTENANCE AND TROUBLESHOOTING 4.1 Overview....................................................................................................19 4.1.1 Water Addition ...............................................................................20 4.2 Fuses ....................................................................................................21 4.3 Electrolyte Replacement............................................................................21 4.
CONTENTS FIGURES 1-1. 1-2. 2-1. 2-2. 2-3. 2-4. 3-1. 3-2. 3-3. 3-4. 3-5. 3-6. 4-1. 4-2. Trace Oxygen Detector Technology........................................................... 2 Trace Oxygen Analyzer Module - Top View............................................... 3 Analyzer Module Interconnection with Instrument Platform ....................... 7 Outline and Mounting Dimensions ............................................................. 8 Back Panel Connections ......................................
PREFACE PURPOSE/SAFETY SUMMARY The purpose of this manual is to provide information concerning the components, functions, installation and maintenance of this particular NGA 2000 module. Some sections may describe equipment not used in your configuration. The user should become thoroughly familiar with the operation of this module before operating it. Read this instruction manual completely.
PREFACE CAUTION: PARTS INTEGRITY Tampering or unauthorized substitution of components may adversely affect safety of this product. Use only factory documented components for repair. CAUTION: HIGH PRESSURE GAS CYLINDERS This analyzer requires use of pressurized gas. See General Precautions for Handling and Storing High Pressure Cylinders, in the rear of this manual. WARNING: CAUSTIC LIQUID The electrolyte is a caustic solution. Review the Material Safety Data Sheet in the rear of this manual.
PREFACE GLOSSARY Analyzer Module The module that contains all sensor/detector components for development of a Primary Variable signal; includes all signal conditioning and temperature control circuitry. Backplane The interconnect circuit board which the Controller Board, Power Supply, Analyzer Module power and network cables, I/O Modules and Expansion Modules plug into. Control Module The Operator Interface plus the Controller Board.
PREFACE Power Supply Any of a variety of components that provides conditioned power to other NGA 2000 components, from the Power Supply Board that plugs into the front of the Backplane in a stand-alone instrument to several larger ones that can power larger collections of modules and components. Primary Variable The measured species concentration value from an Analyzer Module. Secondary Variable Data placed on the network by a module regarding current status, e.g.
PREFACE SPECIFICATIONS - GENERAL MEASUREMENT SPECIES RANGES ACCURACY SENSITIVITY NOISE LINEARITY RESPONSE TIME ZERO DRIFT SPAN DRIFT EFFECT OF TEMPERATURE EFFECT OF FLOW OPERATING TEMPERATURE POWER REQUIREMENTS Trace Oxygen 0 to 100 ppm (output scalable down to 0-2 ppm fullscale) ±3% of reading or ±0.02% of range (except for ranges ≤ 100 ppm: ±3% of reading or ±0.
PREFACE SPECIFICATIONS - PHYSICAL MATERIALS IN CONTACT WITH SAMPLE DIMENSIONS WEIGHT MOUNTING CASE CLASSIFICATION MAX. SEPARATION FROM PLATFORM Stainless steel, Teflon, Delrin, neoprene See Figure 2-2, Outline and Mounting Dimensions 6.8 kg (15 lbs.) Horizontal, external to Platform or custom installed in a panel General Purpose for installation in weather protected area 1600 m (1 mile) SPECIFICATIONS - GAS CONNECTIONS SAMPLE IN 1/4 inch O.D. tube fitting SAMPLE OUT 1/4 inch O.D.
PREFACE CUSTOMER SERVICE, TECHNICAL ASSISTANCE AND FIELD SERVICE For order administration, replacement Parts, application assistance, on-site or factory repair, service or maintenance contract information, contact: Rosemount Analytical Inc. Process Analytical Division Customer Service Center 1-800-433-6076 RETURNING PARTS TO THE FACTORY Before returning parts, contact the Customer Service Center and request a Returned Materials Authorization (RMA) number.
PREFACE DOCUMENTATION The following Trace Oxygen Analyzer Module instruction materials are available. Customer Service or the local representative to order. Contact 748420 Instruction Manual (this document) COMPLIANCES This product may carry approvals from several certifying agencies for use in nonhazardous, indoor locations. If so, the product will carry approval insignia on the product name-rating plate. ® NRT L /C Rosemount Analytical Inc.
INTRODUCTION 1 1.1 OVERVIEW This manual describes the Trace Oxygen (TO2) Analyzer Module of Rosemount Analytical's NGA 2000 Series of gas analysis components. The TO2 Analyzer Module is designed to continuously determine the concentration of trace oxygen in a flowing gaseous mixture. The concentration is expressed in parts-per-million.
1 INTRODUCTION 1.4 FEATURES Among the features included in the TO2 Analyzer Module are: • Quick start feature • Electrolyte level alarm • High oxygen protection circuit with alarm • Sample flow indication. SECONDARY ANODE (+) BI-STRATA™ DIFFUSION BARRIER e- ELECTRONICS S SAMPLE IN KOH O2 - OH O2 SAMPLE OUT S eO2 SENSING CATHODE (-) SECONDARY CATHODE (-) O2 SENSING ANODE (-) FIGURE 1-1.
INTRODUCTION 1 Sensor Assembly Network/Power Module Computer Board Sensor Sample Flow Sensor Power Board FIGURE 1-2.
1 INTRODUCTION NOTES 4 Trace Oxygen Analyzer Module Rosemount Analytical NGA 2000 748420-A August 1999
INSTALLATION 2 2.1 UNPACKING If the Trace Oxygen (TO2) Analyzer Module is received as a separate unit, carefully examine the shipping carton and contents for signs of damage. Immediately notify the shipping carrier if the carton or contents is damaged. Retain the carton and packing material until all components associated with the TO2 Analyzer Module are operational. 2.2 ASSEMBLY Before installation of the TO2 Analyzer Module, electrolyte must be added to the Sensor.
2 INSTALLATION Note Do not add water. The volume and concentration of the bottled electrolyte is premeasured. Reinstall the black Sensor cover and carefully reinstall the Sensor Assembly inside the Analyzer Module. Do not the tilt the Sensor Assembly excessively as electrolyte may leak out. 2.3 LOCATION (See Figure 2.2) The TO2 Analyzer Module comes standard with mounting ears for easy installation on flat, horizontal surfaces.
INSTALLATION 2 Sample The sample must be clean and dry before entering the Analyzer Module. Sample should be filtered for particulates down to two microns, and should have a dew point at least 5 °C (13 °F) below the coldest expected ambient temperature. Pressure Constant between 13.8 and 69 hPa - gauge (0.2 and 1.0 psig) sample inlet pressure is recommended. If a needle valve is used upstream of the Analyzer Module to control flow, the inlet pressure to the needle valve should not exceed 345 hPa (5 psig).
2 INSTALLATION .23 [6] 7.75 [197] 7.75 [197] 1.61 [41] .23 [6] 5.78 [147] .266 DIA [6.75] 18.56 [471] 12.00 [305] 11.00 [279] 6.00 [152] 7.00 [178] 8.25 [206] 8.10 [206] 10.15 [258] 2.70 [68] 6.62 [168] 1.2 [31] .06 [1.5] 1.2 [31] FIGURE 2-2.
INSTALLATION 2 Sample Inlet 1/4" Tube Sample Exhaust 1/4" Tube FIGURE 2-3. BACK PANEL CONNECTIONS CAUTION: GAS OVERPRESSURE At no time should sample, zero or span gas inlet pressure exceed 69 hPa gauge (1.0 psig). Damage to the Sensor may occur if this pressure level is exceeded. CAUTION: SAMPLE FLOW Do not test the sample pressure by blocking the exhaust. When the pressure is released the sudden surge of flow will spin the internal flowmeter off its bearings and destroy it. 2.4.
2 INSTALLATION Network Connections Power Connection Fuse Power Indicator Light FIGURE 2-4. TRACE OXYGEN ANALYZER FRONT PANEL 2.5 ELECTRICAL CONNECTIONS WARNING: ELECTRICAL SHOCK HAZARD Operate this equipment only when covers are secured. Servicing requires access to live parts which can cause death or serious injury. Refer servicing to qualified personnel. For safety and proper performance, this module must be connected to a properly grounded three-wire source of electrical power.
STARTUP AND OPERATION 3 3.1 OVERVIEW Prior to initial startup, the user should perform the leak test procedure outlined in Section 2 For the remainder of this section, Analyzer Module interconnection with a Platform or some interfacing component will be assumed. Display and Keypad information refers to that which the user can expect to see and do with regard to the Front Panel of the Platform.
3 STARTUP AND OPERATION TO2 1 ppm O 2 19.4 0 Range 3 50 Sensor current: 1.4403 mA Sensor temperature: 26.3 C Temperature current: Sample Flow: DISPLAY 2.01 mA 511 ml/min PARMS. MENU NEXT INFO FIGURE 3-1. RUN MODE DISPLAY 3.2.2 MENU DISPLAYS The Menu structure enables the user to access data and functions, and put information onto the network. From the Run Mode display, press the MENUS softkey to gain access to the Main Menu. Main Menu Basic controls . . . Expert controls and set up . . .
STARTUP AND OPERATION 3 The Basic controls menu is as follows: Basic Controls Measurement range number: Range upper limit: Range and functional control: CURRENTRNGHI CONTROL Sleep Mode: Exit Sleep Mode! Initiate Quick Start! Quick Start: HOME ESCAPE INFO FIGURE 3-3. BASIC CONTROLS MENU This menu allows the user to view the current range’s upper limit, Sleep mode, and quick start status. It also allows quick start initiation or exit from sleep mode.
3 STARTUP AND OPERATION Analyzer module set up Range settings . . . Displayed parameters . . . Analyzer tag: HOME TAG ESCAPE INFO FIGURE 3-5. ANALYZER MODULE SET-UP MENU 3.2.3 HELP DISPLAYS The Help structure is intended to be an on-line "tutorial," context-sensitive and topicinterconnected, so that the user can practically operate NGA 2000 without the need of an instruction manual. A typical help menu: Zero/Span calibration help This allows manual control of the zero and span.
STARTUP AND OPERATION 3 3.3 STARTUP PROCEDURE Establish sample or zero gas flow through the analyzer module at a nominal flow rate of 2 SCFH (1 l/min). Allow gas to flow for 15 to 30 seconds before applying power. Apply power to the TO2 Analyzer Module. Upon initial startup, the separate modules, Controller Board and network "self-install." The display shows the progress of the automatic installation routine, together with a button marked RE_INIT.
3 STARTUP AND OPERATION Under the Technical Level Configuration sub-menu, select Diagnostic menus... and then select Analyzer Module Diagnostics…. In the Analyzer Module Diagnostics sub-menu select Calibration Parameters.... In the Advanced/Expert Calibration sub-menu select Gas Scale Factor.... To use the GSF, enter the volumetric percentages of each component present in the sample gas. To view more background components, press the MORE softkey.
STARTUP AND OPERATION 3 5. Press the ← key to return to the previous menu. 6. Introduce a suitable span gas into the SAMPLE INLET and allow reading to stabilize. Move the cursor to the User span calibration... line and press the ↵ key. 7. Move the cursor to the Span gas concentration: line and press the ↵ key. Enter the correct span gas value by using the ↑↓ keys to change value and the ←→ keys to select position. Press the ↵ key to enter the new span gas value. 8.
3 STARTUP AND OPERATION 3.7 ROUTINE OPERATION The TO2 Analyzer Module is designed to analyze the sample stream continuously. Normally, it is never powered off except for servicing or for a prolonged shutdown. Maximum permissible interval between calibration checks depends on the analytical accuracy required, and therefore cannot be specified. Initially, the instrument should be checked at least once every 3-4 months.
MAINTENANCE AND TROUBLESHOOTING 4 4.1 OVERVIEW CAUTION: QUALIFIED PERSONNEL This equipment should not be adjusted or repaired by anyone except properly qualified service personnel. WARNING: PARTS INTEGRITY Tampering with or unauthorized substitution of components may adversely affect safety of this product. Use only factory-approved components for repair. The TO2 Analyzer Module requires very little maintenance during normal operation. The sensor in the TO2 utilizes a liquid electrolyte.
4 MAINTENANCE AND TROUBLESHOOTING Sensor Cover TOP VIEW Indicator, Electrolyte Level Enclosure Back Wall Sensor Reservoir Mounting Screws (2 places) SIDE VIEW Mounting Screws (3 places) Flow Sensor FIGURE 4-1. TRACE OXYGEN ANALYZER SENSOR ASSEMBLY 4.1.1 WATER ADDITION To add water: 1. Remove the top cover of the analyzer module. 2. Unscrew the black sensor cover. 3. Slide the cover back just enough to allow the neck of the fill bottle to fit into the sensor reservoir. 4.
MAINTENANCE AND TROUBLESHOOTING 4 4.2 FUSES Remove power to the Analyzer Module prior to fuse replacement. To replace the Power Fuse, locate the fuse cover on the front panel of the Analyzer Module, as shown partially in Figure 2-3. Push and turn the fuseholder cover 1/4 turn counterclockwise. Remove and replace the fuse as required. There are no other fuses in the Analyzer Module. 4.
4 MAINTENANCE AND TROUBLESHOOTING Install replacement Sensor in reverse order. Check Sensor for leaks and add electrolyte as described in section 2.2.1. Reinstall Sensor Assembly in Analyzer Module and reconnect J5 and J6 to the power board. After installation of new Sensor, it will be necessary to load the new calibration data supplied with the Sensor. Enter the new calibration data by entering the Load Factory Calibration Data menu.
MAINTENANCE AND TROUBLESHOOTING 4 4.6 PRINTED CIRCUIT BOARDS All three printed circuit boards can be replaced, if necessary. Refer to Figure 1-2 for location of the Power, Network and Computer Boards. To remove any PCB, disconnect the associated cables first. Tag each connector and its location before disconnecting any wiring. This helps in reassembly. The Power board and Computer board are located on a common bracket. 4.
4 MAINTENANCE AND TROUBLESHOOTING The TO2 analyzer gives erratic and very insensitive readings. Check to see that the electrolyte level is within the limits indicated on the reservoir. Add distilled water as required. If the level is within limits, the electrolyte may have been contaminated. Refer to section 4.2 above for proper procedure to replace electrolyte.
REPLACEMENT PARTS 5 WARNING: PARTS INTEGRITY Tampering with or unauthorized substitution of components may adversely affect safety of this product. Use only factory-approved components for repair. 5.
5 REPLACEMENT PARTS NOTES 26 Trace Oxygen Analyzer Module Rosemount Analytical NGA 2000 748420-A August 1999
APPENDIX A. TO2 IDENTIFICATION MATRIX A Each analyzer is configured per the customer sales order. Below is the TO2 sales matrix which lists the various configurations available. To identify the configuration of an analyzer, locate the analyzer name-rating plate. The 12position sales matrix identifier number appears on the analyzer name-rating plate.
A APPENDIX A.
APPENDIX B. TO2 MENU STRUCTURE B B.1 INTRODUCTION This Appendix contains a listing of the menus belonging to the TO2 Analyzer Module. It also lists the available configuration elements, and where they are to be found. B.2 TO2 MENUS From the main menu, you can access the three major menu trees. Basic controls…allows access to range number selection and range limit, Quick Start initiation and status, and Sleep Mode status and cancellation.
B APPENDIX B. TO2 MENU STRUCTURE Expert Controls and set up … allows access to the Expert analyzer controls… and Analyzer module set up… sub menus. The Expert Controls menu allows range number and functional control selection. It also shows the range upper and lower limits.
APPENDIX B. TO2 MENU STRUCTURE B The Analyzer Module Setup menu allows access to the Range settings… and Display parameters… sub menus. The Range Settings menu allows configuration of the upper and lower limit of the 4 ranges on the Analyzer Module. The maximum and minimum range limits are shown and adjustment beyond these limits is not allowed.
B APPENDIX B. TO2 MENU STRUCTURE The Displayed parameters are the secondary parameters shown on the Display screen (see figure 3-1). The desired parameters can be selected from this menu. Technical level configuration… provides access to the service and diagnostic menus including calibration, gas scale factor, and sensor factory calibration data.
APPENDIX B. TO2 MENU STRUCTURE B The Analyzer Manufacturing Data screen and Analyzer Module Service History screen are both accessible from the Service menus… sub menu. These screens provide factory set data concerning the configuration of the Analyzer Module.
B APPENDIX B. TO2 MENU STRUCTURE From the Analyzer Diagnostics menu, all analyzer health diagnostic information can be accessed. Calibration controls are also accessible from this menu.
APPENDIX B. TO2 MENU STRUCTURE B The Primary Variable Parameters screen provides details on the sensor, and advises the current status of the sleep mode. If the oxygen concentration exceeds 100 ppm, the sleep mode timer begins counting. At the end of 45 minutes, if the concentration has not dropped below 100 ppm, the Analyzer Module will go into sleep mode to protect the sensor from damage due to high oxygen exposure.
B APPENDIX B. TO2 MENU STRUCTURE It is not recommended to conduct user zero and span calibration functions since the sensor is factory calibrated and does not exhibit detectable degradation of calibration over time. The risk of erroneous calibration due to inaccurate gases is greater than the potential of factory calibration change.
APPENDIX B. TO2 MENU STRUCTURE B The Load Factory Calibration screens allow the user to enter the factory calibration data unique to the sensor in the Analyzer Module. If the sensor is replaced, this data must be entered from the data sheet provided with the replacement sensor. Additional data points can be accessed by pressing the MORE softkey. Calibration Data Display screens look identical to the Load Factory Calibration screens except they are not editable.
B APPENDIX B. TO2 MENU STRUCTURE The Gas Scale Factor screens allow the user to enter in information relating to the background gas of the trace oxygen measurement. The total concentration of all entries must add up to 100 or the unit will not compute the new adjusted gas scale factor.
APPENDIX B. TO2 MENU STRUCTURE B The Physical Measurements screen displays sample flow information as well as electrolyte level validity. Temperature Parameters… selection directs the user to the sensor temperature information. It is recommended that the user not conduct temperature calibration of the sensor in the field.
B APPENDIX B.
APPENDIX C. USER INTERFACE HELP C C.1 USER INTERFACE HELP INSTRUCTIONS This section provides a means of rapidly finding any desired function or configuration factor in the menu system. The NGA menu system is necessarily complex due to the wide variety of configuration possibilities available with the NGA architecture. This section consists of a series of titles describing the function or configuration desired, with a series of menu titles that show the path taken to that function.
C APPENDIX C.
APPENDIX C.
C APPENDIX C.
GENERAL PRECAUTIONS FOR HANDLING AND STORING HIGH PRESSURE GAS CYLINDERS Edited from selected paragraphs of the Compressed Gas Association's "Handbook of Compressed Gases" published in 1981 Compressed Gas Association 1235 Jefferson Davis Highway Arlington, Virginia 22202 Used by Permission 1. Never drop cylinders or permit them to strike each other violently. 2.
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WARRANTY Goods and part(s) (excluding consumables) manufactured by Seller are warranted to be free from defects in workmanship and material under normal use and service for a period of twelve (12) months from the date of shipment by Seller. Consumables, glass electrodes, membranes, liquid junctions, electrolyte, o-rings, etc., are warranted to be free from defects in workmanship and material under normal use and service for a period of ninety (90) days from date of shipment by Seller.
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FIELD SERVICE AND REPAIR FACILITIES Field service and repair facilities are located worldwide. U.S.A. To obtain field service on-site or assistance with a service problem, contact (24 hours, 7 days a week): National Response Center 1-800-654-7768 INTERNATIONAL Contact your local Rosemount Sales and Service office for service support.
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Rosemount Analytical 748377-A MATERIAL SAFETY DATA SHEET Product : Part No.: Distributor : Address: Telephone: ELECTROLYTE1 904676 Rosemount Analytical Inc. 4125 East La Palma Ave., Anaheim, CA 92807-1802 (714) 986-7600 24 HOUR EMERGENCY TELEPHONE NO.
M ATERIAL SAFETY DATA SHEET 748377-A SECTION VI - HEALTH HAZARD DATA Threshold limit value: Routes of Entry: Effects of overexposure : Emergency & First Aid Procedures: NA Inhalation, eyes, skin, ingestion Corrosive to tissue. Inhalation of mist may cause respiratory tract damage, Eyes - Corrosive, immediately flush with water for at least 15 minutes. Call a physician. Skin - Corrosive, remove contaminated clothing. Wash with soap or mild detergent and large amounts of water at least 15 minutes.
INSTRUCTIONS 015-748439-A Rosemount Analytical ADDENDUM TO2 INSTRUCTION MANUAL 748420 This addendum serves as an amendment to the TO2 Instruction Manual 748420. The following information should be considered part of the manual, and supersedes any conflicting information in the body of the manual. Read this information and note the conflicts. MENU DISPLAYS Menu: 0 MAIN Menu: 1 ANALSET Rosemount Analytical Inc.
ADDENDUM Menu: 2 SPAN Menu: 3 SPANI1 Menu: 4 ANALOPI1 2 of 18 Rosemount Analytical August 1999 748439-A
ADDENDUM Menu: 5 ANALSETI1 Menu: 6 AMMAN Menu: 7 AMMANI1 748439-A August 1999 Rosemount Analytical 3 of 18
ADDENDUM Menu: 8 AMSVC Menu: 9 AMSVCI1 Menu: 10 ADIAG 4 of 18 Rosemount Analytical August 1999 748439-A
ADDENDUM Menu: 11 AMPWR Menu: 12 AM1V Menu: 13 ADIAGI1 748439-A August 1999 Rosemount Analytical 5 of 18
ADDENDUM Menu: 14 RANGESETAM Menu: 15 RANGESSETI1 Menu: 16 SPANI2 6 of 18 Rosemount Analytical August 1999 748439-A
ADDENDUM Menu: 17 AMPWRI1 Menu: 18 AM1VI1 Menu: 19 AM2VA 748439-A August 1999 Rosemount Analytical 7 of 18
ADDENDUM Menu: 20 ANALSIMPLE Menu: 21 LINSETI2 Menu: 22 SPANI3 8 of 18 Rosemount Analytical August 1999 748439-A
ADDENDUM Menu: 23 SIMPLEZERO Menu: 24 SIMPLESPANI1 Menu: 25 SIMPLEZEROI1 748439-A August 1999 Rosemount Analytical 9 of 18
ADDENDUM Menu: 26 AMHELPINDEX Menu: 27 AMTRENDI1 Menu: 28 LISTNOTES 10 of 18 Rosemount Analytical August 1999 748439-A
ADDENDUM Menu: 29 MPARMS Menu: 30 DISPLAY Menu: 31 MPARMSI1 748439-A August 1999 Rosemount Analytical 11 of 18
ADDENDUM Menu: 32 SW_DIAG Menu: 33 AM_TMP Menu: 34 ADV_CAL 12 of 18 Rosemount Analytical August 1999 748439-A
ADDENDUM Menu: 35 EXPCTRLI1 Menu: 36 CALI2 Menu: 37 TEMPI1 748439-A August 1999 Rosemount Analytical 13 of 18
ADDENDUM Menu: 38 DISPLAYI1 Menu: 39 AM_TMP_LC Menu: 40 AM_TMP_HC 14 of 18 Rosemount Analytical August 1999 748439-A
ADDENDUM Menu: 41 CAL_FACTORY Menu: 42 CAL_FACTORY1 Menu: 43 DISP_CAL 748439-A August 1999 Rosemount Analytical 15 of 18
ADDENDUM Menu: 44 DISP_CAL1 Menu: 45 GSF Menu: 46 GSF1 16 of 18 Rosemount Analytical August 1999 748439-A
ADDENDUM Menu: 47 UNITS Menu: 48 UNITSI1 Menu: 49 ABOUT 748439-A August 1999 Rosemount Analytical 17 of 18
ADDENDUM Menu: 50 ABOUT1 Menu: 51 ALARM1 Menu: 52 MANDATA 18 of 18 Rosemount Analytical August 1999 748439-A
