User`s manual

44 Chapter 5: Software Description
Calorimetry Sciences Corp.
CSC 5300 N-ITC III 45
User’s Manual
then screw the syringe completely into the buret drive as shown in Figures 5-16 and
5-17.
3. Insert the syringe and burette drive into the N-ITC III as shown in Figure 5-18. Make
sure that the burette key slots line up correctly with the syringe position slot located
towards the front of the N-ITC III. Push the drive completely down and turn clock-
wise to lock in place.
4. Turn on the stirrer at 150 rpm and allow
the system to re-equilibrate until the heat
reading on the calorimeter is stable.
5. Set the parameters for the particular ex-
periment of interest in ITCRun under the
Setup tab (Figure 5-19).
6. Click the Go icon or select
Experiment⇒Start to begin the titration.
While the program is running the
Figure 5-18: Inserting the burette assembly
into the calorimeter.
Figure 5-16: Inserting the syringe into the
burette shaft.
Figure 5-17: Finger-tightening the syringe in
the burette shaft.