Operation Manual ® Syncore Platform 093008 en
Syncore Platform Table of contents Table of contents Read this Operation Manual through carefully before starting to use the Syncore Product Line. Always keep these instructions ready at hand close to the equipment so that they may be consulted quickly at all times. Chapter 2 provides important safety instructions that must be followed to ensure safe ope ration of the unit. We reserve the right to make technical changes without prior notice.
1 Scope of delivery Syncore Platform 1 Scope of delivery 1.1 Configuration Syncore Analyst 1A 0 Voltage 1 100V 50/60Hz 2 120V 50/60Hz 3 230V 50/60Hz Condenser 0 None S Type S, Standard C Type C, Cold trap Round receiving flask, KS 24/20,PLG 0 None 2 2000ml total volume Rack type (incl. vacuum cover) 4 Crystal Rack R-4 Analyst 5 Crystal Rack R-6 Analyst 6 Rack R-12 Analy Residual volume of glass tubes 4 1ml 5 0.
Syncore Platform 1 Scope of delivery 1.2 1P Configuration Syncore Polyvap 000 Voltage 1 100V 50/60Hz 2 120V 50/60Hz 3 230V 50/60Hz Condenser 0 None S Type S, Standard C Type C, Cold trap Round receiving flask, KS 24/20,PLG 0 None 1 1000ml total volume 2 2000ml total volum Rack type (incl. vacuum cover) 0 None 1 Crystal Rack R-4 2 Crystal Rack R-6 3 Rack R-12 4 Standard Rack R-24 5 Falcon Rack R-24 6 Rack R-96 Figure 2: BUCHI Syncore Polyvap R-24 in addition: 1 Power system cable PNE, 1.
1 Scope of delivery Syncore Platform 1.3 Individual components Single Platform Components Syncore Single Platform 230 V 50/60 Hz Syncore Single Platform 120 V 50/60 Hz Syncore Single Platform 100 V 50/60 Hz Order code 38429 38430 38431 Scope of delivery 1 Syncore Single Platform, complete Including: 1 Adjustment wrench for adjusting eccen38477 tricity and unbalance compensation 1 Power system cable PNE, 1.
Syncore Platform 2 Safety 2 Safety This unit and all its components have been built in accordance with the state of the art and recognized safety rules. Nevertheless, certain risks and dangers may be involved when working with the unit or its individual components: • Whenever the unit is not being used in accordance with its intended purpose, or • Whenever the staff operating the unit have not lack sufficient training and know-how. 2.
2 Safety Syncore Platform 2.3 Authorized use This unit has been designed and built as a laboratory instrument.
Syncore Platform 2 Safety • Use of the single platform with sample holders or sample containers that have not been developed for use on the Syncore single platform. • Working at above atmospheric pressure 2.
2 Safety Syncore Platform 2.7 Safety procedures The regional and local laws and regulations must be observed. It is necessary to wear personal protective equipment such as protective goggles, gloves and a laboratory coat. It is only permissible to assemble and dismantle certain parts of the Syncore when such action is necessary to carry out the functional requirements. This activity can be performed manually or by use of the tool which is supplied.
Syncore Platform 3 Function 3 Function Syncore comprises a series of compact, highly versatile instruments suitable for all aspects of parallel synthesis and evaporation. There are three pre-defined assemblies: • Syncore Reactor • Syncore Polyvap • Syncore Analyst The instruments are tailored to the customer’s needs in various applications. The standard configurations can be modified to meet individual requirements by using additional accessories. 3.
3 Function Syncore Platform 3.2 Syncore Analyst R-4, R-6 and R-12 The Syncore Analyst is a prallel work-up station designed go give high productivity. It comprises a basic unit , a rack with residual volume cooling for samples with appropriate glass vessels having residual volume appendices, a vacuum connection and a condenser unit with appropriate receiving flasks .
Syncore Platform 3 Function 3.4 Syncore Polyvap R-4 to R-96 The Syncore Polyvap comprises a single platform , a rack for samples and fitting glasses , a vacuum cover , and a condenser unit with a suitable receiving flask . This configuration can be used to condense different samples simultaneously down to dryness. The samples are shaken in a horizontal vortex movement at up to 300 rpm. The operator can adjust the eccentricity of this vortex movement to suit the working volume at hand.
4 Putting into Operation Syncore Platform 4 4.1 Putting into operation Complete and intact delivery After unpacking the delivery, inspect for any signs of damage. It is important that any damage that may have occurred in transit is recognized at the time of unpacking. If any damage is detected, it is necessary to determine the facts of the situation immediately (to be reported to the postal authorities, railway company or transport agent).
Syncore Platform 4 Putting into Operation 4.4 Function test for drive and speed indicator There should be no objects of any kind resting upon the base plate or between the base-plate and the housing of the equipment. • Set a speed of 60 RPM by turning the speed controller to the right. • The display unit should indicate “60” and the base plate of the basic unit should move slowly without any pronounced vibration.
4 Putting into Operation Syncore Platform 4.6 Attachment of the condenser unit S and C • Screw the right- or left-hand support rod (depending on the work-place or the working procedure) into the hole provided in the rear feet. • Secure the cooler bracket (shackle) to the support rod using the cross sleeve . • Secure the cooler to the shackle. • Attach the transition piece to the cooler with the clamp . • Also secure the receiving vessel to the transition piece with the clamp .
Syncore Platform 5 Operation 5 5.1 Operation The single Platform Ensure that the equipment is properly put into operation according to the recommendations outlined in Chapter 4. The use of racks, vacuum connections, and further accessories enable the device to be used for: • Cooling • Heating • Shaking • Evaporation and • Concentration Figure 12: The single platform The handling of the device is kept simple.
5 Operation Syncore Platform Exceeding the maximum temperature Do not under any circumstances continue using the unit when the temperature displayed is above 155°C. Contact a BUCHI service agent immediately in such a case. Moving parts Various parts of the accessories are accelerated in the horizontal plane to speeds of up to 600 rpm. This means that the machine may cast off parts that have not been fastened correctly and present a risk for the operator and the laboratory equipment.
Syncore Platform 5 Operation 5.3 Figure 13: Display of the basic unit after starting up the equipment Temperature and speed of rotation 1. Press once on the „UP“ or the „DOWN“ button on the temperature control unit. The display shifts from the current temperature to the prescribed set-point tempe rature. 2. Set a new control temperature by repeated pressing of the „UP“-Key. 3.
5 Operation Syncore Platform 5.4 Program mode, temperature/time steps Typical application: • Definition of the temperature and time in several stages at a constant RPM, e.g. in a parallel evaporation at different temperatures. • Repetition of heating cycles for, e.g. material testing cycles Schematic: Programming mode, controlled parameters Figure 14: Display of the basic unit after starting up the equipment 1. Activating the programming function: Press once on the „PROGRAM“ button.
Syncore Platform 5 Operation If the UP-key of the time controller is hold until“to 1” appears, the equipment starts the program again using the 1st program step and the program will repeat indefinitely in a cyclic manner. This step can be interrupted by the user by pressing the „STOP“-Key. 7. Checking the program: Press the „PROGRAM“ button repeatedly and check the parameters in all steps of the program. The display jumps back to step 1 at the end of the program. 8.
5 Operation Syncore Platform 5.5 Further control parameters 5.5.1 Vacuum connection heater The vacuum connection is capable of being heated. This reduces or prevents condensation in the vacuum connection. The heater for the vacuum cover is controlled by the basic platform and can be limited to a given maximum temperature by the operator. The temperature of the vacuum cover is always controlled, regardless of whether the unit is being operated manually or via a program.
Syncore Platform 5 Operation 5.6 Pre-set safety settings Standard pre-set settings The Syncore platform allows specific pre-set safety settings to limit the following operating parameters: • • • • Maximum temperature, either 150°C or 100°C Minimum temperature, either +20°C or –20°C. Rotational speed of the base plate; either 300 or 600 rpm Automatic start of the vortex movement at the previously set rotational speed or at a fixed rotational speed of 60 rpm.
5 Operation Syncore Platform Changing the Pre-Set safety settings For the Syncore Analyst we strongly recommend not to raise the maximum temperature above 100°C, reducing the minimum temperature below +20 °C, or raising the maximum rotational speed above 300 rpm. In special cases, the operator can change these safety settings. The unit must be switched OFF. Use a small screwdriver in the adjustment socket on the back of the unit to change the settings of the various individual switches.
Syncore Platform 5 Operation 5.8 Signal-outputs F1 The Syncore platform is equipped with various signal outlets that significantly extend the functionality of the unit. There are two 24 V valve signal outlets. One is temperature-controlled, the second is controlled by the ending of a program. F4 F5 Figure 17: Signal-outputs and fuses with the corresponding order number qty 10) for the new Syncore setup. Fuse 100 - 120 V F1 15.0 AT (100 V) 051497 16.0 AT (120 V) 041859 F4 3.15 AT 019659 F5 3.
5 Operation Syncore Platform The valve is switched on and off as described below: • The program has not reached its end: Valve open. A coolant curcuits through the condenser unit. • The program has come to an end: Valve open. Cooling water continues to flow through the condenser unit in order to condense any remaining solvent vapors. • 1 Hour (= post-program running time) after the program has ended: Valve closed. The cooling water flow stops as the post-program expires.
Syncore Platform 5 Operation 5.11 Signal inputs The platform also accomodates an analog TTL-signal inlet . An external start or stop signal can be sent to the Syncore single platform across this TTL-inlet. Start signal: If the Syncore single platform is in the program mode, a pre-defined program (temperature / time steps) is started. Otherwise a manually set temperature is activated. Stop signal: If a program has been activated beforehand, that program is stopped.
5 Operation Syncore Platform 5.12 Adjusting the eccentricity Introduction The unit allows an adjustment of the eccentricity of the horizontal shaking movement between 0 and 5 mm. Please note that the moving parts take up more energy when the eccentricity is greater and the rotational speeds must be reduced accordingly.
Syncore Platform 5 Operation ping position of the base plate also brings about an exact positioning of the access used for manual adjustment of the eccentricity. Adjusting eccentricity Never make adjustments while the base plate is still moving. The introduction of the tool into the drive unit while it is still in motion can damage the unit and lead to personal injuries. The base plate must be in the pre-defined stopping position before any new eccentricity of the vortex movement is set.
5 Operation Syncore Platform Checking the setting The new setting must be checked every time the eccentricity has been changed. The tool must be removed from the unit. The vortex movement must not be switched ON while the tool is still in the drive. This could cause damage to the unit and lead to personal injuries. Make a qualitative check by evaluating the swirl in a liquid within a sample tube at the new setting. Adjust the unbalance compensation before checking.
Syncore Platform 5 Operation Adjusting the unbalance compensation Never make any adjustments while the base plate is still moving. Introduction of the tool into the drive unit while it is still moving can damage the unit and cause personal injuries. The base plate must be in its pre-defined stopping position before setting a new unbalance compensation. To ensure this, switch the unit ON and let the base plate rotate at least one full rotation.
5 Operation Syncore Platform Adjusting the unbalance compensation and eccentricity Optimum speed [rpm] Optimum eccentricity [mm] R-4 with vacuum cover 250 4.0 R-6 with vacuum cover 300 Rack with resp. without vacuum cover Unbalance [mm]: insert and turn the des wrench until you reach the value on the adjustment wrench 4.0 4.0 15 27 29 R-6 with residual volume and vacuum cover 300 R-12 with vacuum cover 380 4.0 25 R-12 with residual volume and vacuum covers 380 4.
Syncore Platform 5 Operation 5.14 Trouble-shooting: The single platform Observation Cause Correction Display does not light No power Connect the unit to the power system. Check fuses. Check the power system Display lights only in part Display unit defective Contact BÜCHI service agent Unit does not heat up Heater not turned on Press „START“ Unit does not heat up Heater not turned on Temperature set-point too low; Setpoint temperature higher than room temperature.
6 Maintenance Syncore Platform 6 6.1 Maintenance Cleaning Single platform • Use a cloth dampened in alcohol to clean the housing of the Syncore single platform. If it is severely fouled, a mild detergent and water may be used. • Never use hard brushes to clean the base plate. • If it is severely fouled, the black rubber ring around the base plate may be removed and cleaned with a mild detergent or with alcohol. 6.
Syncore Platform 6 Maintenance 6.3 Routine inspection of the equipment (annually) Temperature control unit The base plate heater is checked by the user or by a BUCHI service agent using an external temperature sensor. For this, introduce a thermocouple Ø 4 mm (see chapter, Replacement parts) into the hole at the side of the base plate and check the temperature of the base plate while it is in a steady state condition: at 50 °C, at 100 °C, and at 150 °C.
6 Maintenance Syncore Platform Activating the calibration mode • The unit must be switched OFF. • To activate the mode for calibration of the unit, press the „STOP“ and „PROGRAM“ buttons simultaneously and switch the unit ON. Continue pressing the two buttons until cross-dashes (— —— ——) appear in the display and a „C“ appears in the Step display. The calibration mode has now been activated. This can be abandoned only by switching the machine OFF and then switching it back ON again.
Syncore Platform 6 Maintenance 6.5 Error messages: Calibration Whenever the progress of the calibration is interrupted by an error, „End“ appears in the temperature display and the pertinent error number appears in the time display. These errors (unlike technical malfunctions of the unit) can be deleted again by pressing a button. The following error messages are possible in the calibration mode: Error No. Description 50 Heating plate too hot. 51 Temp.
6 Maintenance Syncore Platform 6.7 Error No.
Syncore Platform 7 Taking out of Operation 7 Taking out of operation Before the unit and its accessories are transported, all hoses must be removed and internal chambers must be cleaned of all residues of reagents, heating, or cooling agents. All parts must be clean, with no chemicals present on the unit itself or on its accessories. 7.1 Storage / Transport Wherever possible the unit, and its accessories are to be stored and shipped in the original packages. 7.
8 Replacement Parts Syncore Platform 8 Replacement parts Use only genuine BUCHI consumables and spare parts for maintenance and repair to ensure optimum system performance and reliability. Prior written permission of the manufacturer should be obtained before any modifications are made to the spare parts used. 8.1 Description 1 Adjustment wrench 1 Operation Manual German English French Italian Spanish 1 Corner bracket kpl., 1 pcs.
Syncore Platform 9 Appendix 9 9.
9 Appendix Syncore Platform 9.3 FCC requirements (for USA and Canada) English: This equipment has been tested and found to comply with the limits for a Class A digital device, pusuant to both Part 15 of the FCC Rules and the radio interference regulations of the Canadian Department of Communications. These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment.
Syncore Platform 9 Appendix 9.
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