Installation manual

93
1. Type edc and change the following parameters:
• NAME = newexp
• EXPNO = 2
• PROCNO = 1
2. Click on ‘SAVE’
3. Type rpar C13APT all
4. Type lock and select CDCl3 by clicking on it
5. Wait until the locking process is finished, then shim for best homogeneity
6. Type getprosol
7. Click on ‘SAVE’
8. Type xaua
9. Type xaup
10. Correct the phase by making the CH3 and CH carbons of the same phase
and the CH2 and C carbons of opposite phase. The relative phase is
arbitrary.