Installation manual

6.1.2. Creating the parameter file

NOTE: In this case the APT experiment does not exist in the parameter set

library and it has to be created. Since the acquisition and processing of APT

is similar to the DEPT135 experiment, the parameter file C13DEPT135 can

be used as a template for creating the new experiment.

1. Type edc and change the following parameters:

• NAME = newexp

• EXPNO = 1

• PROCNO = 1

2. Click on ‘SAVE’

3. Type rpar C13DEPT135 all

4. Type pulprog jmod

NOTE: The only change necessary in the parameters, is the pulse program.

If desired, number of scans ‘ns’ or relaxation time ‘d1’ may be changed.

5. Type wpar C13APT all

NOTE: The parameter files for C13APT are now stored in the directory

/u/exp/stan/nmr/par and before being added to the experiment list in ICON-

NMR it should be tested on a sample.

6.1.3. Testing the experiment

Sample: ~0.3 M in 0.6 ml CDCl3 of a small organic molecule such as

Cholesterylacetate