Installation manual
73
• ‘Insert New Sample’: a window to change the sample will appear
and a new file name, solvent and experiment can be selected. The
current user stays logged in.
• ‘Use Same / Continue’: The sample stays in the magnet, (locked
and shimmed) and a new experiment can be selected.
NOTE: It is generally better to keep a sample in the magnet if the instrument
will not be used for a long period of time.
5. Automation
NOTE: Automation is designed to run experiments using a variety of sample
changers and can also be used in manual sample change operation allowing
greater flexibility than Routine Spectroscopy (Chapt. 5).
5.1. Experiment setup
NOTE: The following setup examples are simple exercises to demonstrate
the different acquisition methods in ICON-NMR using three samples.
Samples:
~0.3 M in 0.6 ml CDCl3 of a small organic molecule such as Strychnine
~0.3 M in 0.6 ml DMSO of a small organic molecule such as Carvone
~0.3 M in 0.6 ml CDCl3 of a small organic molecule such as Menthol
1. Type iconnmr
2. Click on ‘Automation’
3. Click on ‘Identify User’