Technical data
Table Of Contents
- Contents
- Introduction
- System Description
- Installation
- Overview
- Step 1: Selecting a Location
- Step 2: Unpack and Inspect the Instrument
- Step 3: Set Up the Vacuum Pump
- Step 4: Connect the Power Cord
- Step 5: Install the Dry Compressed Air or O2 Supply
- Step 6: Install the Signal Output Cables
- Step 7: Install the Dual Plasma Burner
- Step 8: Install the Dual Plasma Controller
- Step 9: Install Column Connections
- Step 10: Install the Transfer Line
- Front Panel Controls and Initial Startup
- Operation
- Maintenance
- Pump Maintenance
- Cleaning the Detector
- Changing the Oil Mist Filter (RV5)
- Reaction Cell Cleaning
- Flow Sensor Calibration
- Detector Sensitivity
- Assembling the Dual Plasma Burner for Component Replacement with the SCD
- Assembling the Dual Plasma Burner for Component Replacement with the NCD
- Tube Replacement for the SCD
- Tube Replacement for the NCD
- Troubleshooting
- Index
88 Operation and Maintenance Manual
Flow Sensor Calibration
The hydrogen and oxidant flow sensors installed in the Dual Plasma Controller
have very good repeatability, but significant non-linearity. They have each
been factory calibrated at the midrange flow rate (50 SCCM) using an NIST
traceable flow meter. Over the typical operating range for the SCD, the flow
sensors should produce accuracy of better than ±10% of reading. However,
due to sensor non-linearity at low or high flow extremes, error greater than
this could be observed.
If greater accuracy is desired at a particular flow rate range, it is possible to
re-calibrate the flow sensors. A reference flow meter, appropriate gases, and a
trim-pot adjustment tool are required for this procedure. With the controller
on and no gases flowing, the zero calibration points are set with RP6 and RP4
for the hydrogen and oxidant flow streams, respectively. Connect a reference
flow meter to the gas outlet(s) on the back of the controller. Connect
pressurized gas line(s) to the inlets on the back of the controller. Connect
jumper (JP1) to bypass the pressure fault circuitry. Allow the burner
temperature to exceed 325 °C in order for the hydrogen and oxidant valves to
be open. The spans of the sensors are then adjusted for the particular flow
stream to the desired flow rate as measured with the reference flow meter. The
span adjustments are set with RP3 and RP2, for hydrogen and oxidant
respectively, so that the display on the controller matches the value obtained
with the reference flow meter. Upon completion, remove the reference flow
meter and return the bypass jumper (JP1) to its original position.