Technical data
Table Of Contents
- Contents
- Introduction
- System Description
- Installation
- Overview
- Step 1: Selecting a Location
- Step 2: Unpack and Inspect the Instrument
- Step 3: Set Up the Vacuum Pump
- Step 4: Connect the Power Cord
- Step 5: Install the Dry Compressed Air or O2 Supply
- Step 6: Install the Signal Output Cables
- Step 7: Install the Dual Plasma Burner
- Step 8: Install the Dual Plasma Controller
- Step 9: Install Column Connections
- Step 10: Install the Transfer Line
- Front Panel Controls and Initial Startup
- Operation
- Maintenance
- Pump Maintenance
- Cleaning the Detector
- Changing the Oil Mist Filter (RV5)
- Reaction Cell Cleaning
- Flow Sensor Calibration
- Detector Sensitivity
- Assembling the Dual Plasma Burner for Component Replacement with the SCD
- Assembling the Dual Plasma Burner for Component Replacement with the NCD
- Tube Replacement for the SCD
- Tube Replacement for the NCD
- Troubleshooting
- Index
14 Operation and Maintenance Manual
6 Maintenance
Pump Maintenance 82
Table 3. Operating Life of Components for Edwards RV5 Vacuum Pump 82
Cleaning the Detector 83
Changing the Oil Mist Filter (RV5) 84
Reaction Cell Cleaning 85
Figure 23. Reaction Cell, PMT Housing and PMT Socket 86
Figure 24. Reaction Cell 86
Flow Sensor Calibration 88
Detector Sensitivity 89
Assembling the Dual Plasma Burner for Component Replacement with the SCD 90
Figure 25. Ferrule Placement on Lower Burner Tube 90
Figure 26. Proper Ferrule Orientation to the Large Ceramic Tube 91
Figure 27. Large Ceramic Tube Properly Inserted into the Quartz Heater Assembly 91
Figure 28. Orientation of the Double Taper Ferrule 92
Figure 29. Positioning the Upper Tube in the Union Fitting 92
Figure 30. Tightening the Heater Swivel Nut 93
Figure 31. Proper Alignment of the Burner 93
Assembling the Dual Plasma Burner for Component Replacement with the NCD 95
Figure 32. Ferrule Placement on Lower Burner Tube 95
Figure 33. Proper Ferrule Orientation to the Large Quartz Tube 96
Figure 34. The Quartz Tube Properly Inserted into the Quartz Heater Assembly 96
Figure 35. Burner Assembly Detail 97
Figure 36. Burner Assembly Alignment 97
Tube Replacement for the SCD 98
Figure 37. Orientation of the Double Taper Ferrule 98
Figure 38. Positioning the Upper Tube in the Union Fitting 99
Figure 39. Proper Ferrule Orientation to the Large Ceramic Tube 99
Figure 40. Large Ceramic Tube Properly Inserted into the Quartz Heater Assembly 100
Figure 41. Tightening the Heater Swivel Nut 100
Figure 42. Proper Alignment of the Burner 101
Tube Replacement for the NCD 102
Figure 43. Proper Ferrule Orientation to the Large Quartz Tube 102
Figure 44. Large Quartz Tube Properly Inserted into the Quartz Heater Assembly 103
Figure 45. NCD Tube Replacement Detail 104
Figure 46. NCD Tube Replacement Detail 104