User guide

Chromatographic Checkout 4
Advanced User Guide 83
Final time 2 0 min
Purge time 0.75 min
Purge flow 60 mL/min
Septum purge 3 mL/min
Detector
Temperature 300 °C
H
2
flow 3 mL/min
Air flow 60 mL/min
Makeup flow (N
2
) Makeup + column = 10 mL/min
Output 30 display units (30 pA)
Oven
Initial temp 60 °C
Initial time 0 min
Rate 1 20 °C/min
Final temp 200 °C
Final time 3 min
ALS settings (if installed)
Sample washes 2
Sample pumps 6
Sample wash volume 8
Injection volume 1 µL
Syringe size 10 µL
Solvent A pre washes 2
Solvent A post washes 2
Solvent A wash volume 8
Solvent B pre washes 0
Solvent B post washes 0
Solvent B wash volume 0
Injection mode (7693A) Normal
Airgap Volume (7693A) 0.20
Viscosity delay 0
Table 11 NPD Checkout Conditions (continued)