Specifications

110 5975 Series MSD Troubleshooting and Maintenance Manual
4 General Maintenance
7 Syringe or pipette PFTBA into the vial. With the vial vertical, the liquid
should be just below the end of the internal tube, approximately 70 µL of
sample.
8 Push the calibration vial into the valve as far as possible.
9 Withdraw the vial 1 mm. This prevents damage when you tighten the
collar.
10 Turn the collar clockwise to tighten it.
The collar should be snug but not overly tight. Do not use a tool to tighten
the collar. It does not require that much force.
11 Reinstall the analyzer window cover.
12 Select Purge Calibrant Valve from the Vacuum menu in the Tune and Vacuum
Control view.
CAUTION
Failure to purge the calibration valve will result in damage to the filaments and
detector.